MINUTE SYNTHESIS OF ELECTROPHILIC ALKENES UNDER MICROWAVE IRRADIATION

被引:2
|
作者
ABDALLAHELAYOUBI, S [1 ]
TEXIERBOULLET, F [1 ]
HAMELIN, J [1 ]
机构
[1] UNIV RENNES 1,CNRS,PHYSICOCHIM STRUCT GRP 3,CAMPUS BEAULIEU,F-35042 RENNES,FRANCE
来源
SYNTHESIS-STUTTGART | 1994年 / 03期
关键词
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
Condensation of carbonyl derivatives 2 with active methylene compounds 1 is efficiently achieved, within 3 to 15 minutes under microwave irradiation by a solvent free reaction in the presence of carefully adjusted amounts of piperidine leading to Knoevenagel products 3 in good to excellent yields.
引用
收藏
页码:258 / 260
页数:3
相关论文
共 50 条
  • [21] Synthesis of Polymer Nanocomposites Under Microwave Irradiation
    Bogdal, Dariusz
    Prociak, Aleksander
    Michalowski, Slawomir
    CURRENT ORGANIC CHEMISTRY, 2011, 15 (02) : 178 - 188
  • [22] IMPROVED SYNTHESIS OF OXAZOLINE UNDER MICROWAVE IRRADIATION
    OUSSAID, B
    BERLAN, J
    SOUFIAOUI, M
    GARRIGUES, B
    SYNTHETIC COMMUNICATIONS, 1995, 25 (05) : 659 - 665
  • [23] Synthesis of azoles and diazines under microwave irradiation
    Patel, VM
    Desai, KR
    INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY, 2004, 13 (03) : 283 - 284
  • [24] Synthesis of Substituted Salicylanilides under Microwave Irradiation
    Eva Veverková
    Mária Mečiarová
    Štefan Toma
    Jozef Balko
    Monatshefte für Chemie / Chemical Monthly, 2003, 134 : 1215 - 1219
  • [25] Synthesis and properties of DMDO under microwave irradiation
    Res. Inst. of Indust. and Chem. Eng., South China Univ. of Tech., Guangzhou 510640, China
    Huanan Ligong Daxue Xuebao/Journal of South China University of Technology (Natural Science), 2001, 29 (08): : 7 - 9
  • [26] An improved synthesis of α-carbolines under microwave irradiation
    Vera-Luque, P
    Alajarín, R
    Alvarez-Builla, J
    Vaquero, JJ
    ORGANIC LETTERS, 2006, 8 (03) : 415 - 418
  • [27] SYNTHESIS OF QUINOXALINES UNDER FOCUSED MICROWAVE IRRADIATION
    VILLEMIN, D
    MARTIN, B
    SYNTHETIC COMMUNICATIONS, 1995, 25 (15) : 2319 - 2326
  • [28] Green Synthesis of Aminobisphosphonates Under Microwave Irradiation
    Reddy, G. Chandra Sekhar
    Reddy, M. Veera Narayana
    Reddy, N. Bakthavatchala
    Reddy, C. Suresh
    PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS, 2011, 186 (01) : 74 - 80
  • [29] Improved synthesis of pyridazinediones under microwave irradiation
    Bourel, L
    Tartar, A
    Melnyk, P
    TETRAHEDRON LETTERS, 1996, 37 (24) : 4145 - 4148
  • [30] Synthesis of quinoxalines under focussed microwave irradiation
    Ecole Nat. Superieure d'Ingenieurs, I.S.M.R.A., Groupe Catalyse et Modelisation, F-14050 Caen Cedex, France
    SYNTH. COMMUN., 15 (2319-2326):