SPECTROFLUOROMETRIC FLOW-INJECTION DETERMINATION OF ADRENALINE WITH AN IODINE SOLID-PHASE REACTOR

被引：25
|
作者：
KOJLO, A [1 ]
CALATAYUD, JM [1 ]
机构：
[1] UNIV VALENCIA,DEPT QUIM ANALIT,E-46100 BURJASSOT,SPAIN
来源：
ANALYTICA CHIMICA ACTA | 1995年 / 308卷 / 1-3期
关键词：
FLOW INJECTION; FLUOROMETRY; ADRENALINE HYDROCHLORIDE; PHARMACEUTICAL ANALYSIS;
D O I：
10.1016/0003-2670(94)00656-7
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A novel strategy for the preparation of solid-phase reactors by ''impregnation'' of a poly(vinyl chloride) coil with the reagent was carried out and applied to the fluorimetric flow injection determination of adrenaline. The calibration graph was linear over the range 5-25 mg l(-1) of adrenaline, the reproducibility (R.S.D.) was 1.8% (15 replicates) and the sample throughput 32 h(-1).
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页码：334 / 338
页数：5
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