SPECTROFLUOROMETRIC FLOW-INJECTION DETERMINATION OF ADRENALINE WITH AN IODINE SOLID-PHASE REACTOR

被引:25
|
作者
KOJLO, A [1 ]
CALATAYUD, JM [1 ]
机构
[1] UNIV VALENCIA,DEPT QUIM ANALIT,E-46100 BURJASSOT,SPAIN
关键词
FLOW INJECTION; FLUOROMETRY; ADRENALINE HYDROCHLORIDE; PHARMACEUTICAL ANALYSIS;
D O I
10.1016/0003-2670(94)00656-7
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A novel strategy for the preparation of solid-phase reactors by ''impregnation'' of a poly(vinyl chloride) coil with the reagent was carried out and applied to the fluorimetric flow injection determination of adrenaline. The calibration graph was linear over the range 5-25 mg l(-1) of adrenaline, the reproducibility (R.S.D.) was 1.8% (15 replicates) and the sample throughput 32 h(-1).
引用
收藏
页码:334 / 338
页数:5
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