SPECTROFLUOROMETRIC FLOW-INJECTION DETERMINATION OF ADRENALINE WITH AN IODINE SOLID-PHASE REACTOR

被引:25
|
作者
KOJLO, A [1 ]
CALATAYUD, JM [1 ]
机构
[1] UNIV VALENCIA,DEPT QUIM ANALIT,E-46100 BURJASSOT,SPAIN
关键词
FLOW INJECTION; FLUOROMETRY; ADRENALINE HYDROCHLORIDE; PHARMACEUTICAL ANALYSIS;
D O I
10.1016/0003-2670(94)00656-7
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
A novel strategy for the preparation of solid-phase reactors by ''impregnation'' of a poly(vinyl chloride) coil with the reagent was carried out and applied to the fluorimetric flow injection determination of adrenaline. The calibration graph was linear over the range 5-25 mg l(-1) of adrenaline, the reproducibility (R.S.D.) was 1.8% (15 replicates) and the sample throughput 32 h(-1).
引用
收藏
页码:334 / 338
页数:5
相关论文
共 50 条
  • [1] Flow-Injection Spectrophotometric Determination of Captopril Exploiting Silver Chloranilate Solid-Phase Reactor
    Suarez, Willian Toito
    Bonifacio, Viviane Gomes
    Madi, Alexandro Alves
    Fatibello-Filho, Orlando
    ANALYTICAL LETTERS, 2009, 42 (07) : 973 - 988
  • [2] CERIUM(IV) ARSENITE AS A SOLID-PHASE REACTOR FOR USE IN FLOW-INJECTION ANALYSIS - SPECTROPHOTOMETRIC DETERMINATION OF PROMETHAZINE
    CALATAYUD, JM
    MATEO, VG
    ANALYTICA CHIMICA ACTA, 1992, 264 (02) : 283 - 289
  • [3] Solid-phase reactor with copper(II) phosphate for flow-injection spectrophotometric determination of aspartame in tabletop sweeteners
    Fatibello-Filho, O
    Marcolino, LH
    Pereira, AV
    ANALYTICA CHIMICA ACTA, 1999, 384 (02) : 167 - 174
  • [4] Flow-injection solid-phase spectrophotometry for the determination of zinc in pharmaceutical preparations
    Teixeira, LSG
    Rocha, FRP
    Korn, M
    Reis, BF
    Ferreira, SLC
    Costa, ACS
    ANALYTICA CHIMICA ACTA, 1999, 383 (03) : 309 - 315
  • [5] SOLID-PHASE REACTORS IN FLOW-INJECTION ANALYSIS
    DECASTRO, MDL
    TRAC-TRENDS IN ANALYTICAL CHEMISTRY, 1992, 11 (04) : 149 - 155
  • [6] Solid-phase reactor flow-injection on-line oxidizing spectrofluorimetry for determination and dissolution studies of folic acid
    Zhi-Qi Zhang
    Ying Tang
    Analytical and Bioanalytical Chemistry, 2005, 381 : 932 - 936
  • [7] Solid-phase reactor flow-injection on-line oxidizing spectrofluorimetry for determination and dissolution studies of folic acid
    Zhang, ZQ
    Tang, Y
    ANALYTICAL AND BIOANALYTICAL CHEMISTRY, 2005, 381 (04) : 932 - 936
  • [8] Flow-injection spectrophotometric determination of dipyrone in pharmaceutical formulations using a solid-phase reactor with copper(II) phosphate
    Bonifacio, Viviane G.
    Fatibello Filho, Orlando
    Marcolino-Junior, Luiz H.
    CENTRAL EUROPEAN JOURNAL OF CHEMISTRY, 2013, 11 (11): : 1830 - 1836
  • [9] FLOW-INJECTION SOLID-PHASE CHEMILUMINESCENT IMMUNOASSAY USING A MEMBRANE-BASED REACTOR
    LIU, HJ
    YU, JC
    BINDRA, DS
    GIVENS, RS
    WILSON, GS
    ANALYTICAL CHEMISTRY, 1991, 63 (07) : 666 - 669