Preparation and crystal structural characterization of Cu(II) complex with piperidine-4-carboxylic acid

被引：0

作者：

J. X. Yang

Z. Zhang

Y. P. Tian

J. Y. Wu

Q. L. Liu

A. Usman

S. Chantrapromma

H. K. Fun

机构：

[1] Anhui University,Department of Chemistry

[2] USTC,Department of Chemistry

[3] University Sains Malaysia,X

来源：

Russian Journal of Coordination Chemistry | 2005年 / 31卷

关键词：

Oxygen; Hydrogen; Copper; Reflection; Hydrogen Bond;

D O I：

暂无

中图分类号：

学科分类号：

摘要：

Copper(II) complex with piperidine-4-carboxylic acid (HPipe-4), Cu(HPipe-4)4(ClO4)2 (I) was prepared and characterized by IR, X-ray diffraction, and thermal analysis. The crystal is orthorhombic with space group Ccca, Z = 8, a =17.415(3) Å, b =17.399(2) Å, c = 21.426(3) Å. The copper atom has a square surrounding and is coordinated by four carboxylato oxygen atoms in monodentate coordination mode. Full-matrix least-squares refinements gave a final R value of 0.0723 for 22169 reflections. The complex consists of two perpendicularly arranged molecules differing slightly in conformations and shows a three-dimensional polymeric structure formed by hydrogen bonds.

引用

页码：282 / 285

页数：3

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