Structural characterization of a novel self-assembly heterohexanuclear complex: [Ni2Ag4(μ-dppm)4(pymt)6](SbF6)2 · 2DMF · H2O

被引：0
|
作者：
Hong-wu Xu
Lin Pin
Jin-xia Li
Zhong-ning Chen
Ji-gui Wu
机构：
[1] ZhongYuan University of Technology,Department of Materials and Chemical Engineering
[2] Fujian Institute of Research on the Structure of Matter,Department of Chemistry
[3] Chinese Academy of Sciences,undefined
[4] Lanzhou University,undefined
来源：
Transition Metal Chemistry | 2007年 / 32卷
关键词：
MeCN; Silver Atom; Dppm; Diphenylphosphino; Diphosphines;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
A novel heterohexanuclear complex [Ni2Ag4(μ-dppm)4(pymt)6](SbF 6)2 · 2DMF · H2O (1), was synthesized by self-assembly with [Ag2(μ-dppm)2(MeCN)2](SbF6) 2 and [Et4N][Ni(pymt)3] (dppm = bis(diphenylphosphino)methane, pymt = pyrimidine-2-thiolate) as components and characterized by IR spectra, elemental analysis, 1H-NMR spectrum, 31P-NMR spectrum and Visible-Ultraviolet spectrum. Structure of the complex was determined by X-ray analysis.
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页码：781 / 783
页数：2
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