Synthesis of 5(6)-(4-Aminophenythio)-2-aminobenzimidazole Derivatives: III. Preparation Procedure for 3,4,4'-Triaminodiphenyl Sulfide

被引：0
|
作者：
V. S. Pilyugin
L. V. Yakovleva
机构：
[1] Academy of Sciences of Bashkortostan Republic,Research Istitute of Technology for Herbicides and Plant Growth Regulators
来源：
Russian Journal of Organic Chemistry | 2002年 / 38卷
关键词：
Iron; Chloride; Sulfide; Hydrate; Organic Chemistry;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
A procedure for preparation of 3,4,4'-triaminodiphenyl sulfide by reduction of 4-amino-3,4'-dinitrodiphenyl sulfide with hydrazine hydrate in butanol catalyzed by a mixture of iron(III) chloride and activated carbon was developed providing the product in no less than 80% yield with the main compound content no less than 93%.
引用
收藏
页码：1137 / 1141
页数：4
相关论文
共 50 条
  • [31] SERIES OF 2,4,6-TRINITROTHIOPHENOL DERIVATIVES .67. OXIDATION REACTION OF 3,3'-DIMETHYL-2,4,6,2',4',6'-HEXANITRO DIPHENYL SULFIDE
    SHARNIN, GP
    NURGATIN, VV
    ZHURNAL ORGANICHESKOI KHIMII, 1972, 8 (07): : 1493 - &
  • [32] The synthesis and resolution of 2,2′-, 4,4′-, and 6,6′-substituted chiral biphenyl derivatives for application in the preparation of chiral materials
    Montoya-Pelaez, Pedro J.
    Uh, Yoon-Seo
    Lata, Christopher
    Thompson, Matthew P.
    Lemieux, Robert P.
    Crudden, Cathleen M.
    JOURNAL OF ORGANIC CHEMISTRY, 2006, 71 (16): : 5921 - 5929
  • [33] Pentamethylcyclopentadienylselenium derivatives III. Synthesis and 77Se NMR spectroscopy of bis(pentamethylcyclopentadienyl) polyselenides, Sen(C5Me5)2 (n = 2, 3, 4)
    J Organomet Chem, 1-2 (193):
  • [34] PREPARATION OF [2',3',5',6'-H-2(4)]PTEROYLGLUTAMIC ACID
    DUEKER, SR
    JONES, AD
    SMITH, GM
    CLIFFORD, AJ
    JOURNAL OF LABELLED COMPOUNDS & RADIOPHARMACEUTICALS, 1995, 36 (10): : 981 - 991
  • [35] Synthesis of new pyrido[2′,3′:3,4]pyrazolo[5,1-c]-[1,2,4]triazin-4(6H)-one derivatives
    S. M. Ivanov
    L. M. Mironovich
    L. A. Rodinovskaya
    A. M. Shestopalov
    Russian Chemical Bulletin, 2017, 66 : 1126 - 1130
  • [36] Synthesis of new pyrido[2',3':3,4]pyrazolo[5,1-c]-[1,2,4]triazin-4(6H)-one derivatives
    Ivanov, S. M.
    Mironovich, L. M.
    Rodinovskaya, L. A.
    Shestopalov, A. M.
    RUSSIAN CHEMICAL BULLETIN, 2017, 66 (06) : 1126 - 1130
  • [37] Synthesis of (±)-(3R*, 4S*, 4aR*)-4,8-dihydroxy-3-methyl-3,4,4a,5-tetrahydro-1H-2-benzopyran-1-one
    Uchida, K
    Watanabe, H
    Kitahara, T
    HETEROCYCLES, 2000, 53 (03) : 539 - +
  • [38] Synthesis of Novel 4ʹ-Hydroxy-2ʹ,3-diaryl-3,4,4ʹ,5ʹ-tetrahydro-2H,2ʹH,6H-spiro[thiazolo[3,2-a][1,3,5]triazine-7,3ʹ-thiophen]-6-one Derivatives via Sulfa-Michael/Aldol Cascade Reactions
    Sha Li
    Jiaxi Tan
    Xiaofang Li
    Russian Journal of General Chemistry, 2021, 91 : 128 - 132
  • [39] Preparation of 4-R-5-oxo-6-phenil-1,2,4-triazine-3-sulfochlorides and their derivatives
    Mironovich, L.M.
    Ukrainskij Khimicheskij Zhurnal, 1998, 64 (3-4): : 46 - 48
  • [40] Tris(3-Fluorophenyl)antimony Derivatives (3-FC6H4)3Sb(OC6H3Br2-2,4)2, (3-FC6H4)3Sb(OC6Cl5-2,3,4,5,6)2, and (3-FC6H4)3Sb[OC(O)C6H4(NO2-2)]2: Synthesis and Structure
    Sharutin, V. V.
    Sharutina, O. K.
    Efremov, A. N.
    Andreev, P. V.
    RUSSIAN JOURNAL OF INORGANIC CHEMISTRY, 2018, 63 (02) : 174 - 179
12345