New complexes of 4-[(4-fluorophenyl)amino]-4-oxobut-2-enoic acid with selected transition metal ions: Synthesis, thermal, and magnetic properties

被引：0
|
作者：
W. Ferenc
P. Sadowski
B. Tarasiuk
B. Cristóvão
D. Osypiuk
J. Sarzyński
机构：
[1] Maria Curie-Skłodowska University,Faculty of Chemistry, Department of General and Coordination Chemistry
[2] Maria Curie-Skłodowska University,Institute of Physics
来源：
Russian Journal of General Chemistry | 2017年 / 87卷
关键词：
4-[(4-fluorophenyl)amino]-4-oxobut-2-enoic acid; selected 3; - and 4; -metals; IR and X-ray spectra; thermal stability; magnetic properties;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
Complexes of 4-[(4-fluorophenyl)amino]-4-oxobut-2-enoic acid, HL, with Mn(II), Co(II), Ni(II), Cu(II), Nd(III), Gd(III), and Er(III) were synthesized and characterized by various physico-chemical methods: elemental analysis, FT-IR, TG, DTG, DSC, TG/FT-IR, XRF, XRD, and magnetic measurements using the Gouy’s method and a SQUID-VSM magnetometer. The complexes were found to be hydrates (except Er(III) complex) containing 1 to 4 molecules of water. The carboxylate groups acted as bidentate ligands.
引用
收藏
页码：2719 / 2727
页数：8
相关论文
共 50 条
  • [41] Synthesis and Analgesic Activity of Etyl 4-[(4-Aryl-2-hydroxy-4-oxobut-2-enoyl)amino]benzoates
    Gein, V. L.
    Romanova, A. V.
    Bobrovskaya, O. V.
    Nazarets, O. V.
    Makhmudov, R. R.
    Gradova, E. V.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2022, 92 (11) : 2231 - 2234
  • [42] Synthesis, crystal structure, Hirshfeld surface analysis, DFT and NBO study of ethyl 1-(4-fluorophenyl)-4-[(4-fluorophenyl)amino]-2,6-diphenyl-1,2,5,6-tetrahydropyridine-3-carboxylate
    Bansal, Ravi
    Butcher, Ray J.
    Gupta, Sushil K.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2023, 79 : 877 - +
  • [43] The influence of substitutes on the room temperature photoluminescence of 2-amino-4-oxobut-2-enoic acid molecular crystals
    Gunina, Ekaterina
    Zhestkij, Nikolaj
    Bachinin, Semyon
    Fisenko, Sergey P.
    Shipilovskikh, Daria A.
    Milichko, Valentin A.
    Shipilovskikh, Sergei A.
    PHOTONICS AND NANOSTRUCTURES-FUNDAMENTALS AND APPLICATIONS, 2022, 48
  • [44] New complexes of 3,4-dimethoxyphenylacetic acid with selected transition metal ions: Spectral, thermal, and magnetic properties
    W. Ferenc
    D. Osypiuk
    B. Cristóvão
    J. Sarzyński
    H. Głuchowska
    Russian Journal of General Chemistry, 2017, 87 : 2045 - 2055
  • [45] New complexes of 3,4-dimethoxyphenylacetic acid with selected transition metal ions: Spectral, thermal, and magnetic properties
    Ferenc, W.
    Osypiuk, D.
    Cristovao, B.
    Sarzynski, J.
    Gluchowska, H.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2017, 87 (09) : 2045 - 2055
  • [46] Synthesis, crystal structures, molecular docking, in vitro monoamine oxidase-B inhibitory activity of transition metal complexes with 2-{4-[bis (4-fluorophenyl)methyl]piperazin-1-yl} acetic acid
    Yang, Dan-dan
    Wang, Riu
    Zhu, Jin-long
    Cao, Qi-Yue
    Qin, Jie
    Zhu, Hai-liang
    Qian, Shao-song
    JOURNAL OF MOLECULAR STRUCTURE, 2017, 1128 : 493 - 498
  • [47] Ethyl 2-amino-6-(4-bromophenyl)-4-(4-fluorophenyl)cyclohexa-1,3-diene-1-carboxylate
    Narayana, B.
    Sapnakumari, M.
    Jasinski, Jerry P.
    Fraiser, Peter M.
    Yathirajan, H. S.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1473 - +
  • [48] Spectral characterisation and electrochemical investigation of some divalent transition metal complexes of di(4-fluorophenyl)carbazone
    Siddalingaiah, AHM
    Naik, SG
    Sherigara, BS
    Swamy, BEK
    JOURNAL OF MOLECULAR STRUCTURE-THEOCHEM, 2002, 582 : 69 - 75
  • [49] Synthesis and crystal structure of 2-amino-3-cyano-4-(4-fluorophenyl)-4H-benzo[h]chromene
    Shi, DQ
    Zhuang, QY
    Tu, SJ
    Wang, XS
    CHINESE JOURNAL OF STRUCTURAL CHEMISTRY, 2003, 22 (06) : 713 - 716
  • [50] Complexes of the selected transition metal ions with 4-methoxycinnamic acidPhysico-chemical properties
    Wiesława Ferenc
    Beata Cristóvão
    Jan Sarzyński
    Paweł Sadowski
    Journal of Thermal Analysis and Calorimetry, 2012, 110 : 739 - 748
12345