New complexes of 3,4-dimethoxyphenylacetic acid with selected transition metal ions: Spectral, thermal, and magnetic properties

被引：0
|
作者：
Ferenc, W. [1 ]
Osypiuk, D. [1 ]
Cristovao, B. [1 ]
Sarzynski, J. [2 ]
Gluchowska, H. [1 ]
机构：
[1] Marie Curie Sklodowska Univ, Fac Chem, PL-20031 Lublin, Poland
[2] Marie Curie Sklodowska Univ, Inst Phys, PL-20031 Lublin, Poland
来源：
RUSSIAN JOURNAL OF GENERAL CHEMISTRY | 2017年 / 87卷 / 09期
关键词：
3,4-dimethoxyphenylacetic acid; transition metals; magnetic properties; thermal stability; powder diffraction; OXYGEN STRETCHING FREQUENCIES; CARBOXYLATE COORDINATION; CRYSTAL-STRUCTURE; CU(II) COMPLEXES; 1,10-PHENANTHROLINE; DIMETHOXYPHENYLETHYLAMINE; TETRAHYDROPAPAVERINE;
D O I：
10.1134/S1070363217090213
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
3,4-Dimethoxyphenylacetates of Mn(II), Co(II), Ni(II), Cu(II), and Zn(II) of general formula M(C10H11O4)(2)center dot nH(2)O, where n = 1, 2 or 4 depending on M(II) ions, are obtained. The complexes crystallize in monoclinic or triclinic systems. The carboxylate groups act as bidentate chelating or bridging ligands. On heating in the air (293-1173 K) they decompose in three steps finally forming oxides of the corresponding metals(II) or their mixtures. Magnetic moments of compounds were determined in the ranges of 76-303 and 4-300 K.
引用
收藏
页码：2045 / 2055
页数：11
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