Determination of ginkgolide A, B, and bilobalide in biloba L. extracts by microdialysis-HPLC

被引：0
|
作者：
Houn-Lin Chiu
Hui-Ya Lin
Thomas Ching-Cherng Yang
机构：
[1] National Kaohsiung Normal University,Department of Chemistry
来源：
Analytical and Bioanalytical Chemistry | 2004年 / 379卷
关键词：
High-performance liquid chromatography; Microdialysis; Ginkgolide A; Ginkgolide B; Bilobalide;
D O I：
暂无
中图分类号：
学科分类号：
摘要：
A method has been developed for measuring ginkgolide A, B, and bilobalide in ginkgo biloba L. extracts by using a self-assembled microdialysis device coupled on-line to high-performance liquid chromatography. The optimal conditions for dialysis efficiency and chromatographic analysis were investigated. The results show that the dialysis efficiencies for ginkgolide A, B, and bilobalide are 97.8–100.4%. For the spike concentration of 45 mg L−1, the recoveries of ginkgolide A, B, and bilobalide in ginkgo biloba L. extracts were at 97–100.7% with 3.1–4.7% RSD. The proposed method has therefore been shown to be applicable to the analysis of ginkgolide A, B, and bilobalide in ginkgo biloba L. extracts.
引用
收藏
页码：445 / 448
页数：3
相关论文
共 50 条
  • [41] Development and Validation of Liquid Chromatography-mass Spectrometry Method for the Determination of Intracellular Concentration of Ginkgolide A, B, C, and Bilobalide in Transporter-Expressing Cells
    Yaro, Peter
    Nie, Jing
    Xu, Mingcheng
    Zeng, Kui
    Zeng, Su
    CURRENT PHARMACEUTICAL ANALYSIS, 2020, 16 (06) : 763 - 773
  • [42] Determination of Hypericin in St. John's Wort (Hypericum perforatum L.) extracts using HPLC-ED
    Sofic, E.
    Janicijevic, Copra A.
    Maksimovic, M.
    Tahirovic, I
    Klepo, L.
    Topcagic, A.
    Huseinovic, S.
    Vidic, D.
    Cavar, S.
    Kroyer, G.
    PLANTA MEDICA, 2011, 77 (12) : 1256 - 1256
  • [43] Determination of fruit chemical properties of Morus nigra L., Morus alba L. and Morus rubra L. by HPLC
    Gundogdu, M.
    Muradoglu, F.
    Sensoy, R. I. Gazioglu
    Yilmaz, H.
    SCIENTIA HORTICULTURAE, 2011, 132 : 37 - 41
  • [44] Ginkgolic acids in Ginkgo biloba L. leaf TCM extracts: Simultaneous HPLC quantification of all five derivatives using ginkgoneolic acid as a single marker compound
    Kuchta, K.
    Wang, R.
    Lin, Y.
    Rauwald, H. W.
    Fang, L.
    Qiao, H.
    Kobayashi, Y.
    PLANTA MEDICA, 2014, 80 (16) : 1524 - 1524
  • [45] Characterization ofMatricaria recutita L. Flower extracts by HPLC-MS and HPLC-DAD analysis
    N. Mulinacci
    A. Romani
    P. Pinelli
    F. F. Vincieri
    D. Prucher
    Chromatographia, 2000, 51 : 301 - 307
  • [46] HPLC evaluation of water-soluble extracts of Chamaenerion angustifolium L. and Pentaphylloides fruticosa L
    Shikov, A. N.
    Poltanov, E.
    Pozhoritskaya, O.
    Dormon, H. J. D.
    Makarov, V
    Tikhonov, V
    Hiltunen, R.
    PLANTA MEDICA, 2007, 73 (09) : 916 - 917
  • [47] Characterization of Matricaria recutita L. flower extracts by HPLC-MS and HPLC-DAD analysis
    Prucher, D., 2000, Friedr. Vieweg und Sohn Verlags GmbH (51) : 5 - 6
  • [48] Determination of antioxidant and antimicrobial activities of Rumex crispus L. extracts
    Yildirim, A
    Mavi, A
    Kara, AA
    JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2001, 49 (08) : 4083 - 4089
  • [49] HPLC screening of phenolic compounds in winter savory (Satureja montana L.) extracts
    Cetkovic, Gordana S.
    Mandic, Anamarija I.
    Canadanovic-Brunet, Jasna M.
    Djilas, Sonja M.
    Tumbas, Vesna T.
    JOURNAL OF LIQUID CHROMATOGRAPHY & RELATED TECHNOLOGIES, 2007, 30 (02) : 293 - 306
  • [50] Comparison of Two Ginkgo biloba L. Extracts on Oxidative Stress and Inflammation Markers in Human Endothelial Cells
    Piazza, Stefano
    Pacchetti, Barbara
    Fumagalli, Marco
    Bonacina, Fabrizia
    Dell'Agli, Mario
    Sangiovanni, Enrico
    MEDIATORS OF INFLAMMATION, 2019, 2019
12345