Effects of the Nature of Transition Metal on the Composition and Structure of Reaction Products of M[(OOCC5H4)Mn(CO)3]2[O(H)Me]4 (М = Cu(II), Ni(II), Co(II), or Mn(II)) with 1,10-Phenanthroline

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作者：
A. A. Grineva
M. A. Uvarova
R. R. Datchuk
S. E. Nefedov
机构：
[1] Russian Academy of Sciences,Kurnakov Institute of General and Inorganic Chemistry
来源：
Russian Journal of Inorganic Chemistry | 2018年 / 63卷
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摘要：
Reactions of M[(OOCC5H4)Mn(CO)3]2[O(H)Me]4 (M = Ni(II), Co(II), or Mn(II)) adducts with 1,10-phenanthroline in chloroform at room temperature are found to yield complexes PhennM[(OOCC5H4) Mn(CO)3]2 (Co(II) or Mn(II), n = 2; M = Ni(II), n = 3). A similar reaction of dimeric Cu2[μ-(OOCC5H4) Mn(CO)3]4[O(H)Me]2 yields mononuclear PhenCu[(OOCC5H4)Mn(CO)3][O(H)Me] · MeOH. The resulting complexes are isolated in high yields and characterized by chemical analysis, IR spectroscopy, and X-ray crystallography.
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页码：610 / 617
页数：7
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