Simultaneous Quantitation of Boric Acid and Calcium Fructoborate in Dietary Supplements by HPTLC-Densitometry

被引：0
|
作者：
Andrei Biţă
George Dan MogoŞanu
Ludovic Everard Bejenaru
Carmen Nicoleta Oancea
Cornelia Bejenaru
Octavian Croitoru
Gabriela Rău
Johny NeamŢu
Iulia Daria Scorei
Ion Romulus Scorei
John Hunter
Brad Evers
Boris Nemzer
Florin Anghelina
Otilia-Constantina Rogoveanu
机构：
[1] University of Medicine and Pharmacy of Craiova,Department of Pharmacognosy & Phytotherapy, Faculty of Pharmacy
[2] University of Medicine and Pharmacy of Craiova,Department of Physics, Faculty of Pharmacy
[3] University of Medicine and Pharmacy of Craiova,Department of Vegetal & Animal Biology, Faculty of Pharmacy
[4] University of Medicine and Pharmacy of Craiova,Department of Drug Control, Faculty of Pharmacy
[5] University of Medicine and Pharmacy of Craiova,Department of Organic Chemistry, Faculty of Pharmacy
[6] BioBoron Research Institute,Department of Otorhinolaryngology, Faculty of Medicine
[7] University of Craiova,Department of Physical Medicine and Rehabilitation, Faculty of Medicine
[8] VDF FutureCeuticals,undefined
[9] University of Medicine and Pharmacy of Craiova,undefined
[10] University of Medicine and Pharmacy of Craiova,undefined
来源：
Analytical Sciences | 2017年 / 33卷
关键词：
Boric acid; calcium fructoborate; dietary supplements; HPTLC;
D O I：
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中图分类号：
学科分类号：
摘要：
The paper describes a new, simple, selective and precise high-performance thin-layer chromatographic (HPTLC) method for the simultaneous identification and quantitative determination of boric acid (BA) and calcium fructoborate (CFB) in bulk and tablet/capsule dosage forms of dietary supplements. HPTLC silica gel G 60 F254 precoated glass plates were used as the stationary phase. The mobile phase consisted of 2-propanol-water 8:2 (v/v). The two boron-based compounds were adequately separated with the Rf values of 0.83 ± 0.01 (BA) and 0.59 ± 0.01 (CFB).
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页码：743 / 746
页数：3
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