Simultaneous Quantitation of Boric Acid and Calcium Fructoborate in Dietary Supplements by HPTLC-Densitometry

被引：10

作者：

Bita, Andrei ^{[1
]}

Mogosanu, George Dan ^{[1
]}

Bejenaru, Ludovic Everard ^{[1
]}

Oancea, Carmen Nicoleta ^{[2
]}

Bejenaru, Cornelia ^{[3
]}

Croitoru, Octavian ^{[4
]}

Rau, Gabriela ^{[5
]}

Neamtu, Johny ^{[2
]}

Scorei, Iulia Dania ^{[6
]}

Scorei, Ion Romulus ^{[6
]}

Hunter, John ^{[7
]}

Evers, Brad ^{[7
]}

Nemzer, Boris ^{[7
]}

Anghelina, Florin ^{[8
]}

Rogoveanu, Otilia-Constantina ^{[9
]}

机构：

[1] Univ Med & Pharm Craiova, Fac Pharm, Dept Pharmacognosy & Phytotherapy, 2 Petru Rares St, Craiova 200349, Romania

[2] Univ Med & Pharm Craiova, Fac Pharm, Dept Phys, 2 Petru Rares St, Craiova 200349, Romania

[3] Univ Med & Pharm Craiova, Fac Pharm, Dept Vegetal & Anim Biol, 2 Petru Rares St, Craiova 200349, Romania

[4] Univ Med & Pharm Craiova, Dept Drug Control, Fac Pharm, 2 Petru Rares St, Craiova 200349, Romania

[5] Univ Med & Pharm Craiova, Fac Pharm, Dept Organ Chem, 2 Petru Rares St, Craiova 200349, Romania

[6] Univ Craiova, BioBoron Res Inst, Mircesti St,Bldg M4-1-1, Craiova 200506, Romania

[7] VDF FutureCeuticals, 2692 N State Rt 1-17, Momence, IL 60954 USA

[8] Univ Med & Pharm Craiova, Fac Med, Dept Otorhinolaryngol, 2 Petru Rares St, Craiova 200349, Romania

[9] Univ Med & Pharm Craiova, Fac Med, Dept Phys Med & Rehabil, 2 Petru Rares St, Craiova 200349, Romania

来源：

ANALYTICAL SCIENCES | 2017年 / 33卷 / 06期

关键词：

Boric acid; calcium fructoborate; dietary supplements; HPTLC; BORON; HEALTH; BONE;

D O I：

10.2116/analsci.33.743

中图分类号：

O65 [分析化学];

学科分类号：

070302 ; 081704 ;

摘要：

The paper describes a new, simple, selective and precise high-performance thin-layer chromatographic (HPTLC) method for the simultaneous identification and quantitative determination of boric acid (BA) and calcium fructoborate (CFB) in bulk and tablet/capsule dosage forms of dietary supplements. HPTLC silica gel G 60 F-254 precoated glass plates were used as the stationary phase. The mobile phase consisted of 2-propanol-water 8:2 (v/v). The two boron-based compounds were adequately separated with the R-f values of 0.83 +/- 0.01 (BA) and 0.59 +/- 0.01 (CFB).

引用

页码：743 / 746

页数：4

共 23 条

[1] Simultaneous Quantitation of Boric Acid and Calcium Fructoborate in Dietary Supplements by HPTLC-Densitometry
Andrei Biţă
George Dan MogoŞanu
Ludovic Everard Bejenaru
Carmen Nicoleta Oancea
Cornelia Bejenaru
Octavian Croitoru
Gabriela Rău
Johny NeamŢu
Iulia Daria Scorei
Ion Romulus Scorei
John Hunter
Brad Evers
Boris Nemzer
Florin Anghelina
Otilia-Constantina Rogoveanu
[J]. Analytical Sciences, 2017, 33 : 743 - 746
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[4] HPTLC-Densitometry Method for Simultaneous Determination of Major Lignans and Flavonoids in Podophyllum hexandrum
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[8] Simultaneous Quantitation of Nicotinamide Riboside and Nicotinamide in Dietary Supplements via HPTLC-UV with Confirmation by Online HPTLC-ESI-MS
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[J]. ACTA CHROMATOGRAPHICA, 2020, 32 (02) : 128 - 133
[9] Application of LC and HPTLC-Densitometry for the Simultaneous Determination of Two Multicomponent Mixtures Containing Pyridoxine Hydrochloride and Cyanocobalamine
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[J]. ACTA CHROMATOGRAPHICA, 2013, 25 (03) : 431 - 450
[10] Development and validation of an HPTLC-densitometry method for assay of glucosamine of different forms, in dietary supplement tablets and capsules
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[J]. ACTA CHROMATOGRAPHICA, 2005, 15 : 119 - 130

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