Determination of Organochlorine Pesticides Residue in Ginseng Root by Orthogonal Array Design Soxhlet Extraction and Gas Chromatography

被引:9
|
作者
Lan Quan
Shufen Li
Songjiang Tian
Hong Xu
Anqing Lin
Long Gu
机构
[1] Tianjin University,State Key Laboratory of C1 Chemical Technology School of Chemical Engineering & Technology
[2] Tianjin Entry-Exit Inspection and Quarantine Bureau of the P. R. China,undefined
来源
Chromatographia | 2004年 / 59卷
关键词
Gas chromatography; Soxhlet extraction; Orthogonal array design; Organochlorine pesticides residue; Ginseng;
D O I
暂无
中图分类号
学科分类号
摘要
Organochlorine pesticides are known to enter plant products from contamination via spillage and volatilization of the residues from pesticide-treated soils or storage. A method involving four-factor-three-level orthogonal array design including extracting solvent component, particle size, solvent overflow recycle and time needed for the optimization of extracting nine organochlorine pesticides from ginseng root was developed using Soxhlet extraction followed by capillary gas chromatography–electron capture detection and mass spectrometric confirmation. The extraction conditions were optimized from the experimental data. Relationship between the bioaccumulation of benzenehexachloride isomers and their polarity is discussed based on experimental results.
引用
收藏
页码:89 / 93
页数:4
相关论文
共 50 条
  • [41] Determination of organochlorine pesticides in sediment using graphitized carbon black solid-phase extraction and gas chromatography/mass spectrometry
    Kim, Min-Sun
    Kang, Tae Woo
    Pyo, Heesoo
    Yoon, Junheon
    Choi, Kyunghee
    Hong, Jongki
    JOURNAL OF CHROMATOGRAPHY A, 2008, 1208 (1-2) : 25 - 33
  • [42] Determination of Chlorinated Pesticides in Soil by Solid Phase Extraction–Gas Chromatography
    Mohammad A. Mottaleb
    Mohammad Z. Abedin
    Analytical Sciences, 1999, 15 : 283 - 288
  • [43] Orthogonal array design experiments for optimizing the separation of nine pesticides by micellar electrokinetic chromatography
    Zhang, YP
    Li, XJ
    Yuan, ZB
    Lu, YQ
    MICROCHEMICAL JOURNAL, 2002, 73 (03) : 307 - 315
  • [44] Application of isotope dilution gas chromatography-mass spectrometry in analysis of organochlorine pesticide residues in ginseng root
    Chan, Serena
    Kong, Mei-Fong
    Wong, Yiu-Chung
    Wong, Siu-Kay
    Sin, Della W. M.
    JOURNAL OF AGRICULTURAL AND FOOD CHEMISTRY, 2007, 55 (09) : 3339 - 3345
  • [45] Multi-residue analysis of 18 organochlorine pesticides in 10 traditional Chinese medicines by gas chromatography (GC)
    Sun, Nan
    Hao, Lili
    Xue, Jian
    Jin, Hongyu
    Tian, Jingai
    Lin, Ruichao
    JOURNAL OF HEALTH SCIENCE, 2007, 53 (04) : 464 - 469
  • [46] Residue analysis of organophosphorus and organochlorine pesticides in fatty matrices by gas chromatography coupled with electron-capture detection
    Park, Jae-Woo
    Abd El-Aty, A. M.
    Lee, Myoung-Heon
    Song, Sung-Ok
    Shim, Jae-Han
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION C-A JOURNAL OF BIOSCIENCES, 2006, 61 (5-6): : 341 - 346
  • [47] Bursting bubble flow microextraction combined with gas chromatography for determination of organochlorine pesticides in aqueous samples
    Tazarv, Maryam
    Faraji, Hakim
    Moghimi, Ali
    Azizinejad, Fariborz
    MICROCHEMICAL JOURNAL, 2022, 181
  • [48] Simultaneous Determination of the Organochlorine and Pyrethroid Pesticides in Drinking Water by Single Drop Microextraction and Gas Chromatography
    Carlos, Elenice A.
    Alves, Renata D.
    de Queiroz, Maria Eliana L. R.
    Neves, Antonio A.
    JOURNAL OF THE BRAZILIAN CHEMICAL SOCIETY, 2013, 24 (08) : 1217 - 1227
  • [49] Determination of organochlorine pesticides in propolis by gas chromatography–electron capture detection using double column series solid-phase extraction
    Fang Chen
    Lanzhen Chen
    Qiang Wang
    Jinhui Zhou
    Xiaofeng Xue
    Jing Zhao
    Analytical and Bioanalytical Chemistry, 2009, 393 : 1073 - 1079
  • [50] Determination of Organochlorine Pesticides and Polychlorinated Biphenyls in Surface Water Using Accelerate Solvent Extraction Coupling with Gas Chromatography-Mass Spectrometry
    Shao Yang
    Yang Guo-Sheng
    Han Shen
    Ma Ling-Ling
    Luo Min
    Liu Wei-Hua
    Xu Dian-Dou
    CHINESE JOURNAL OF ANALYTICAL CHEMISTRY, 2016, 44 (05) : 698 - 706