Determination of Organochlorine Pesticides Residue in Ginseng Root by Orthogonal Array Design Soxhlet Extraction and Gas Chromatography

被引:9
|
作者
Lan Quan
Shufen Li
Songjiang Tian
Hong Xu
Anqing Lin
Long Gu
机构
[1] Tianjin University,State Key Laboratory of C1 Chemical Technology School of Chemical Engineering & Technology
[2] Tianjin Entry-Exit Inspection and Quarantine Bureau of the P. R. China,undefined
来源
Chromatographia | 2004年 / 59卷
关键词
Gas chromatography; Soxhlet extraction; Orthogonal array design; Organochlorine pesticides residue; Ginseng;
D O I
暂无
中图分类号
学科分类号
摘要
Organochlorine pesticides are known to enter plant products from contamination via spillage and volatilization of the residues from pesticide-treated soils or storage. A method involving four-factor-three-level orthogonal array design including extracting solvent component, particle size, solvent overflow recycle and time needed for the optimization of extracting nine organochlorine pesticides from ginseng root was developed using Soxhlet extraction followed by capillary gas chromatography–electron capture detection and mass spectrometric confirmation. The extraction conditions were optimized from the experimental data. Relationship between the bioaccumulation of benzenehexachloride isomers and their polarity is discussed based on experimental results.
引用
收藏
页码:89 / 93
页数:4
相关论文
共 50 条
  • [31] Multiresidue determination of organophosphorus and organochlorine pesticides in human biological fluids by capillary gas chromatography
    Pitarch, E
    López, FJ
    Serrano, R
    Hernández, F
    FRESENIUS JOURNAL OF ANALYTICAL CHEMISTRY, 2001, 369 (06): : 502 - 509
  • [32] Residue analysis of selected organophosphorus and organochlorine pesticides in commercial tomato fruits by gas chromatography mass spectrometry
    Wondimu, Kokob Teshome
    Geletu, Abiyot Kelecha
    HELIYON, 2023, 9 (03)
  • [33] Decontamination of organochlorine pesticides in Radix Codonopsis by supercritical fluid extractions and determination by gas chromatography
    Zhao, Chunjie
    Hao, Guiming
    Li, Huanxin
    Luo, Xu
    Chen, Yingjie
    BIOMEDICAL CHROMATOGRAPHY, 2006, 20 (09) : 857 - 863
  • [34] Multi-residue determination of organophosphorus and organochlorine pesticides in environmental samples using solid-phase extraction with cigarette filter followed by gas chromatography-mass spectrometry
    Fang, Guozhen
    Chen, Wen
    Yao, Yunping
    Wang, Junping
    Qin, Junyan
    Wang, Shuo
    JOURNAL OF SEPARATION SCIENCE, 2012, 35 (04) : 534 - 540
  • [35] Hybrid Field-Assisted Solid-Liquid-Solid Dispersive Extraction for the Determination of Organochlorine Pesticides in Tobacco with Gas Chromatography
    Zhou, Ting
    Xiao, Xiaohua
    Li, Gongke
    ANALYTICAL CHEMISTRY, 2012, 84 (01) : 420 - 427
  • [36] DETERMINATION OF 8 ORGANOCHLORINE PESTICIDES AT LOW NANOGRAM LITER CONCENTRATIONS IN GROUNDWATER USING FILTER DISK EXTRACTION AND GAS-CHROMATOGRAPHY
    TOMKINS, BA
    MERRIWEATHER, R
    JENKINS, RA
    BAYNE, CK
    JOURNAL OF AOAC INTERNATIONAL, 1992, 75 (06) : 1091 - 1099
  • [37] Solid phase extraction/gas chromatography/electron capture detector method for the determination of organochlorine pesticides in wildlife and wildlife food sources
    Volz, SA
    Johnston, JJ
    JOURNAL OF SEPARATION SCIENCE, 2002, 25 (03): : 119 - 124
  • [38] Solid phase extraction gas chromatography/electron capture detector method for the determination of organochlorine pesticides in wildlife whole blood.
    Volz, SA
    Johnston, JJ
    Griffin, DL
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2000, 220 : U49 - U49
  • [39] Determination of organochlorine pesticides and chlorobenzenes in strawberries by using accelerated solvent extraction combined with sorptive enrichment and gas chromatography/mass spectrometry
    Wennrich, L
    Popp, P
    Köller, G
    Breuste, J
    JOURNAL OF AOAC INTERNATIONAL, 2001, 84 (04) : 1194 - 1201
  • [40] Simultaneous Determination of Residues of Organochlorine and Pyrethroid Pesticides in Tea by Microwave Assisted Extraction Solid Phase Microextraction-Gas Chromatography
    Yuan Ning
    Yu Binbin
    Zhang Maosheng
    Zeng Jingbin
    Chen Xi
    CHINESE JOURNAL OF CHROMATOGRAPHY, 2006, 24 (06) : 636 - 640