Synthesis of mesityl-substituted 1,3,4-oxadiazoles from mesitotrichloride and aromatic and heteroaromatic acid hydrazides

被引：0
|
作者：
Belen'kii L.I. [1 ]
Luiksaar S.I. [1 ]
Krayushkin M.M. [1 ]
机构：
[1] N. D. Zelinskii Institute of Organic Chemistry
来源：
Chemistry of Heterocyclic Compounds | 1999年 / 35卷 / 4期
关键词：
Mass Spectrum; Organic Chemistry; Hydrazide; Acid Hydrazide; Reductive Condensation;
D O I：
10.1007/BF02319340
中图分类号：
学科分类号：
摘要：
At interaction of 2,4,6-trimethylbenzotrichloride with aromatic (heteroaromatic) acid hydrazides in a mixture of 2,6-lutidine and tert-butanol the processes of alcoholysis and reductive condensation are suppressed. The corresponding 2-aryl- or 2-hetaryl-5-mesityl-1,3,4-oxadiazoles are obtained in high yields. The PMR, IR, and mass spectra of the products are studied. ©1999 KluwerAcademic/Plenum Publishers.
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收藏
页码：492 / 498
页数：6
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