Structure of Thiacalix[4]crown-5 Derivative

被引：0
|
作者：
Zhao, Jiang-Lin [1 ]
Jiang, Xue-Kai [1 ]
Mu, Lan [1 ]
Zeng, Xi [1 ]
机构：
[1] Guizhou Univ, Key Lab Macrocycl & Supramol Chem Guizhou Prov, Guiyang 550025, Peoples R China
来源：
ASIAN JOURNAL OF CHEMISTRY | 2010年 / 22卷 / 08期
关键词：
Thiacalixarene; Crown ether; X-Ray structure;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The single crystal of 1,3-alternate-25,27-bis(2-phthalimidoethoxy) thiacalix[4]crown-5 (1) was obtained by recrystallization from its chloroform-methanol (2:1 v/v) solution. Its structure was confirmed by single crystal X-ray analysis. It crystallizes in the triclinic system (space group, P-1) and the chloroform solvent molecular occupies interstitial lattice space between two calixarene molecules. It displays 1,3-alternate conformation. The crystal packing is-stabilized by weak C-H center dot center dot center dot pi contacts.
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收藏
页码：6613 / 6615
页数：3
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