Structure of Thiacalix[4]crown-5 Derivative

被引：0
|
作者：
Zhao, Jiang-Lin [1 ]
Jiang, Xue-Kai [1 ]
Mu, Lan [1 ]
Zeng, Xi [1 ]
机构：
[1] Guizhou Univ, Key Lab Macrocycl & Supramol Chem Guizhou Prov, Guiyang 550025, Peoples R China
来源：
ASIAN JOURNAL OF CHEMISTRY | 2010年 / 22卷 / 08期
关键词：
Thiacalixarene; Crown ether; X-Ray structure;
D O I：
暂无
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The single crystal of 1,3-alternate-25,27-bis(2-phthalimidoethoxy) thiacalix[4]crown-5 (1) was obtained by recrystallization from its chloroform-methanol (2:1 v/v) solution. Its structure was confirmed by single crystal X-ray analysis. It crystallizes in the triclinic system (space group, P-1) and the chloroform solvent molecular occupies interstitial lattice space between two calixarene molecules. It displays 1,3-alternate conformation. The crystal packing is-stabilized by weak C-H center dot center dot center dot pi contacts.
引用
收藏
页码：6613 / 6615
页数：3
相关论文
共 50 条
  • [31] STRUCTURE OF 4-SULPHONYLAMIDOBENZO-15-CROWN-5
    SIMONOV, YA
    MALINOWSKY, ST
    RUDKEVICH, DM
    KALCHENKO, VI
    KRISTALLOGRAFIYA, 1991, 36 (04): : 887 - 891
  • [32] Tightly connected calix[4]pyrrole/calix[4]crown-5 conjugates: Models for ditopic ion-pair recognition and salt container
    Lee, Chang-Hee
    Lee, Mee-Ja
    Kim, Jong Seung
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 2007, 233
  • [33] Characterization of a Self-Assembled Monolayer Based on a Calix[4]Crown-5 Derivate: Fabrication of a Chemical Sensor Sensitive to Calcium
    Marques de Oliveira, Isabel A.
    Vocanson, Francis
    Uttaro, Jean-Pierre
    Asfari, Zouhair
    Mills, Christopher A.
    Samitier, Josep
    Errachid, Abdelhamid
    JOURNAL OF NANOSCIENCE AND NANOTECHNOLOGY, 2010, 10 (01) : 413 - 420
  • [34] [M(II)([15]CROWN-5)(L)2]++COMPLEXES - THE INFLUENCE OF THE CROWN ETHER CAVITY ON THE MOBILITY OF THE LIGANDS-L
    DICKERT, FL
    GMEINER, W
    FEIGL, M
    ZEITSCHRIFT FUR NATURFORSCHUNG SECTION B-A JOURNAL OF CHEMICAL SCIENCES, 1988, 43 (12): : 1551 - 1555
  • [35] Molecular recognition of protonated polyamines at calix[4]crown-5 self-assembled monolayer modified electrodes by impedance measurements
    Park, Jin-Young
    Kim, Byung-Cheol
    Park, Su-Moon
    ANALYTICAL CHEMISTRY, 2007, 79 (05) : 1890 - 1896
  • [36] Voltammetric studies for cation recognition with thiacalix[4]crown-6s
    Kim, Tae Hyun
    Kim, Jong Seung
    Kim, Hasuck
    JOURNAL OF ELECTROANALYTICAL CHEMISTRY, 2008, 615 (02) : 103 - 109
  • [37] Metal ion shuttling mechanism through thiacalix[4]crown: a computational study
    Hong, Jooyeon
    Cho, Sunhee
    Ham, Sihyun
    TETRAHEDRON LETTERS, 2012, 53 (15) : 2009 - 2012
  • [38] Silver ion shuttling in the trimer-mimic thiacalix[4]crown tube
    Kim, SK
    Lee, JK
    Lee, SH
    Lim, MS
    Lee, SW
    Sim, WB
    Kim, JS
    JOURNAL OF ORGANIC CHEMISTRY, 2004, 69 (08): : 2877 - 2880
  • [39] Synthesis, Crystal Structure, and Vibrational Spectra of an Azomethine Derivative of Benzo-15-crown-5, N-(4′-Benzo-15-crown-5)-5-bromo-2-hydroxyphenylaldimine
    L. Kh. Minacheva
    I. S. Ivanova
    E. N. Pyatova
    A. V. Dorokhov
    A. V. Bicherov
    A. S. Burlov
    A. D. Garnovskii
    V. S. Sergienko
    A. Yu. Tsivadze
    Doklady Chemistry, 2004, 395 : 68 - 73
  • [40] Synthesis, crystal structure, and vibrational spectra of an azomethine derivative of benzo-15-crown-5, N-(4′-benzo-15-crown-5)-5-bromo-2-hydroxyphenylaldimine
    Minacheva, LK
    Ivanova, IS
    Pyatova, EN
    Dorokhov, AV
    Bicherov, AV
    Burlov, AS
    Garnovskii, AD
    Sergienko, VS
    Tsivadze, AY
    DOKLADY CHEMISTRY, 2004, 395 (4-6) : 68 - 73
12345