Discrimination and Characterization of the Volatile Organic Compounds in Schizonepetae Spica from Six Regions of China Using HS-GC-IMS and HS-SPME-GC-MS

被引：15
|
作者：
Li, Chao [1 ]
Wan, Huiying [1 ]
Wu, Xinlong [1 ]
Yin, Jiaxin [1 ]
Zhu, Limin [2 ]
Chen, Hanjiang [2 ]
Song, Xinbo [1 ,3 ,4 ]
Han, Lifeng [3 ,4 ]
Yang, Wenzhi [3 ,4 ]
Yu, Heshui [1 ,2 ,3 ]
Li, Zheng [1 ,2 ,3 ]
机构：
[1] Tianjin Univ Tradit Chinese Med, Coll Pharmaceut Engn Tradit Chinese Med, Tianjin 301617, Peoples R China
[2] Tianjin Univ Tradit Chinese Med, Teaching Hosp 1, Tianjin 300193, Peoples R China
[3] Tianjin Univ Tradit Chinese Med, Haihe Lab Modern Chinese Med, Tianjin 301617, Peoples R China
[4] Tianjin Univ Tradit Chinese Med, State Key Lab Component Based Chinese Med, Tianjin 301617, Peoples R China
来源：
MOLECULES | 2022年 / 27卷 / 14期
基金：
中国国家自然科学基金;
关键词：
volatile organic compounds; Schizonepetae Spica; HS-SPME-GC-MS; HS-GC-IMS; OPLS-DA; TENUIFOLIA;
D O I：
10.3390/molecules27144393
中图分类号：
Q5 [生物化学]; Q7 [分子生物学];
学科分类号：
071010 ; 081704 ;
摘要：
Volatile organic compounds (VOCs) are the main chemical components of Schizonepetae Spica (SS), which have positive effects on the quality evaluation of SS. In this study, HS-SPME-GC-MS (headspace solid-phase microextraction-gas chromatography-mass spectrometry) and HS-GC-IMS (headspace-gas chromatography-ion mobility spectrometry) were performed to characterize the VOCs of SS from six different regions. A total of 82 VOCs were identified. In addition, this work compared the suitability of two instruments to distinguish SS from different habitats. The regional classification using orthogonal partial least squares discriminant analysis (OPLS-DA) shows that the HS-GC-IMS method can classify samples better than the HS-SPME-GC-MS. This study provided a reference method for identification of the SS from different origins.
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页数：16
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