Hydrothennal synthesis and characterization of nanocrystalline PZT powders

被引：54
|
作者：
Deng, Y
Liu, L
Cheng, Y
Nan, CW [1 ]
Zhao, SJ
机构：
[1] Tsing Hua Univ, Dept Mat Sci & Engn, Beijing 100084, Peoples R China
[2] Jiamusi Univ, Sch Mat Engn, Jiamusi 154000, Heilongjiang, Peoples R China
来源：
MATERIALS LETTERS | 2003年 / 57卷 / 11期
关键词：
PZT; nanostructures; hydrothermal synthesis;
D O I：
10.1016/S0167-577X(02)01050-9
中图分类号：
T [工业技术];
学科分类号：
08 ;
摘要：
In this paper, nano-sized lead zirconate-titanate (PZT) powders were synthesized without using any excess lead content by a hydrothermal method based on the reaction of TiO2, Pb(NO3)(2), ZrOCl2.8H(2)O or Zr(NO3)(4).5H(2)O and KOH at 160 degreesC for 4 h. The powders were characterized by X-ray diffraction (XRD) and transmission electron microscopy (TEM). The PZT powder consists of nearly homogenous and spherical grains with an average diameter of 5-10 nm. A possible formation mechanism is proposed. (C) 2002 Elsevier Science B.V. All rights reserved.
引用
收藏
页码：1675 / 1678
页数：4
相关论文
共 50 条
  • [1] Hydrothermal synthesis and characterization of nanocrystalline PZT powders
    Liu Haitao
    Cao Maosheng
    Zhou Yongqiang
    Liang Xiaojuan
    Li Longtu
    RARE METAL MATERIALS AND ENGINEERING, 2008, 37 : 730 - 733
  • [2] Synthesis and characterization of nanocrystalline PZT powders: From sol to dense ceramics
    Mirzaei, Ali
    Bonyani, Maryam
    Torkian, Shahab
    PROCESSING AND APPLICATION OF CERAMICS, 2016, 10 (01) : 9 - 16
  • [3] Synthesis and crystallization of anisotropic shaped ZrO2 nanocrystalline powders by hydrothennal process
    Noh, HJ
    Seo, DS
    Kim, H
    Lee, JK
    MATERIALS LETTERS, 2003, 57 (16-17) : 2425 - 2431
  • [4] Synthesis and Characterization of Nanocrystalline PZT Powders by a Simple Sol-Gel Method
    Zhang, Shaopeng
    Wang, Xiaohui
    Li, Longtu
    HIGH-PERFORMANCE CERAMICS VII, PTS 1 AND 2, 2012, 512-515 : 147 - 152
  • [5] Hydrothermal synthesis and characterization of nanocrystalline ceria powders
    Park, J
    Kim, J
    Han, J
    Nam, SW
    Lim, TH
    JOURNAL OF INDUSTRIAL AND ENGINEERING CHEMISTRY, 2005, 11 (06) : 897 - 901
  • [6] Synthesis and characterization of nanocrystalline niobium nitride powders
    Li, YG
    Gao, L
    JOURNAL OF THE AMERICAN CERAMIC SOCIETY, 2003, 86 (07) : 1205 - 1207
  • [7] CHARACTERIZATION AND SINTERING OF PZT POWDERS
    CHO, SH
    HIREMATH, BV
    BIGGERS, JV
    AMERICAN CERAMIC SOCIETY BULLETIN, 1982, 61 (08): : 818 - 818
  • [8] SYNTHESIS AND CHARACTERIZATION OF NANOCRYSTALLINE POWDERS OF PURE NICKEL AND COPPER
    LIN, HM
    HSIEH, SH
    LEE, PY
    LAI, MS
    WU, JS
    MATERIALS CHEMISTRY AND PHYSICS, 1993, 34 (3-4) : 205 - 213
  • [9] Preparation and characterization of nanocrystalline titania powders by sonochemical synthesis
    Duvarci, Ozlem Caglar
    Ciftcioglu, Muhsin
    POWDER TECHNOLOGY, 2012, 228 : 231 - 240
  • [10] Synthesis and characterization of nanocrystalline RuO2 powders
    Music, S
    Popovic, S
    Maljkovic, M
    Saric, A
    MATERIALS LETTERS, 2004, 58 (09) : 1431 - 1436
12345