Synthesis and structure of the coordination polymer [Li5/3H1/3(H4chhc)]

被引：0
|
作者：
Aliev, S. B. [1 ]
Samsonenko, D. G. [1 ,2 ]
Fedin, V. P. [1 ,2 ]
机构：
[1] Russian Acad Sci, Siberian Branch, AV Nikolaev Inst Inorgan Chem, Novosibirsk 630090, Russia
[2] Novosibirsk State Univ, Novosibirsk 630090, Russia
来源：
RUSSIAN CHEMICAL BULLETIN | 2014年 / 63卷 / 04期
基金：
俄罗斯基础研究基金会;
关键词：
lithium; coordination polymers; metal-organic frameworks; cyclohexanehexacarboxylic acid; X-ray crystallography; METAL; HYDROGEN; STORAGE; DESIGN;
D O I：
10.1007/s11172-014-0539-1
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The coordination polymer of the composition [Li5/3H1/3(H(4)chhc)] was synthesized by the reaction of lithium hydroxide monohydrate with 1,2,3,4,5,6-cyclohexanehexacarboxylic acid (H(6)chhc) at 100 degrees C in a 1,4-dioxane-methanol mixture. The structure of this compound was determined by X-ray crystallography and confirmed by IR spectroscopy, as well as by thermogravimetric and elemental analysis. The coordination polymer has a structure of a 3D metal-organic framework built from lithium cations and H(4)chhc(2-) anions.
引用
收藏
页码：997 / 1000
页数：4
相关论文
共 50 条
  • [41] 1,1′,3,3′,5,5′-Hexamethylspiro[furo[2,3-d]pyrimidine-6(5H),5′-pyrimidine]-2,2′,4,4′,6′(1H,3H,1′H,3′H,5′H)-pentaone
    Pesyan, Nader Noroozi
    Rastgar, Saeed
    Hosseini, Yaser
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O1444 - U3327
  • [42] SYNTHESIS OF 3-HEPTYL-2,4(1H,3H)-QUINOLINEDIONES AND 3-NONYL-2,4(1H,3H)-QUINOLINEDIONES
    LASCHOBER, R
    STADLBAUER, W
    LIEBIGS ANNALEN DER CHEMIE, 1990, (11): : 1083 - 1086
  • [43] Synthesis, Crystal Structure and DFT Studies of 1,3-Dimethyl-5-propionylpyrimidine-2,4,6(1H,3H,5H)-trione
    Sharma, Anamika
    Jad, Yahya E.
    Ghabbour, Hazem A.
    de la Torre, Beatriz G.
    Kruger, Hendrik G.
    Albericio, Fernando
    El-Faham, Ayman
    CRYSTALS, 2017, 7 (01)
  • [44] A new 3D cadmium coordination polymer containing 3-amino-1H-1,2,4-triazole: Synthesis, structure, and property
    Liu, Bing
    Wen, Mei-Ting
    Shen, Mei-Lin
    Miao, Wei-Ni
    He, Ting-Ting
    Xu, Ling
    INORGANIC CHEMISTRY COMMUNICATIONS, 2018, 88 : 38 - 41
  • [45] A new coordination compound based on 3, 3′-bis(1H-tetrazol-5-yl)-4, 4′-azofurazan (H2BTZAF): Preparation, crystal structure, and thermal properties
    Wei, Chenli
    Guo, Zeyu
    Li, Yongjie
    Huang, Jie
    JOURNAL OF MOLECULAR STRUCTURE, 2022, 1250
  • [46] Synthesis of 2,4,6(1H,3H,5H)-pyrimidinetrione-5-carboxaldehyde
    Erkin, A. V.
    Krutikov, V. I.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2010, 80 (03) : 551 - 552
  • [47] Synthesis of 2,4,6(1H,3H,5H)-pyrimidinetrione-5-carboxaldehyde
    A. V. Erkin
    V. I. Krutikov
    Russian Journal of General Chemistry, 2010, 80 : 551 - 552
  • [48] SYNTHESIS OF 5-ARYLIDENE-2,4,6(1H,3H,5H)PYRIMIDINETRIONE DERIVATIVES
    PROUSEK, J
    COLLECTION OF CZECHOSLOVAK CHEMICAL COMMUNICATIONS, 1993, 58 (12) : 3014 - 3016
  • [49] Crystal structure of 3-ferrocenyl-1-phenyl-1H-pyrrole, [Fe(eta(5)-(C5H4C4H3NPh)-C-c)(eta(5)-C5H5)]
    Pfaff, Ulrike
    Korb, Marcus
    Lang, Heinrich
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2016, 72 : 92 - +
  • [50] Synthesis of 5-phosphoryl-substituted 1,3,4(3H)-thiadiazolones
    Kozlov, M. A.
    Volkova, Y. A.
    Zavarzin, I. V.
    RUSSIAN CHEMICAL BULLETIN, 2019, 68 (11) : 2105 - 2107
12345