Synthesis and structure of the coordination polymer [Li5/3H1/3(H4chhc)]

被引：0

作者：

Aliev, S. B. ^{[1
]}

Samsonenko, D. G. ^{[1
,2
]}

Fedin, V. P. ^{[1
,2
]}

机构：

[1] Russian Acad Sci, Siberian Branch, AV Nikolaev Inst Inorgan Chem, Novosibirsk 630090, Russia

[2] Novosibirsk State Univ, Novosibirsk 630090, Russia

来源：

RUSSIAN CHEMICAL BULLETIN | 2014年 / 63卷 / 04期

基金：

俄罗斯基础研究基金会;

关键词：

lithium; coordination polymers; metal-organic frameworks; cyclohexanehexacarboxylic acid; X-ray crystallography; METAL; HYDROGEN; STORAGE; DESIGN;

D O I：

10.1007/s11172-014-0539-1

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

The coordination polymer of the composition [Li5/3H1/3(H(4)chhc)] was synthesized by the reaction of lithium hydroxide monohydrate with 1,2,3,4,5,6-cyclohexanehexacarboxylic acid (H(6)chhc) at 100 degrees C in a 1,4-dioxane-methanol mixture. The structure of this compound was determined by X-ray crystallography and confirmed by IR spectroscopy, as well as by thermogravimetric and elemental analysis. The coordination polymer has a structure of a 3D metal-organic framework built from lithium cations and H(4)chhc(2-) anions.

引用

页码：997 / 1000

页数：4

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