Full-field X-ray diffraction microscopy using polymeric compound refractive lenses

被引:17
|
作者
Hilhorst, J. [1 ]
Marschall, F. [2 ]
Thi, T. N. Tran [1 ]
Last, A. [2 ]
Schuelli, T. U. [1 ]
机构
[1] ESRF, ID 01, F-38043 Grenoble 9, France
[2] KIT, D-76344 Eggenstein Leopoldshafen, Germany
关键词
STRAIN; TOPOGRAPHY; RESOLUTION; NANOSCALE; CATALYST; CONTRAST;
D O I
10.1107/S1600576714021256
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
Diffraction imaging is the science of imaging samples under diffraction conditions. Diffraction imaging techniques are well established in visible light and electron microscopy, and have also been widely employed in X-ray science in the form of X-ray topography. Over the past two decades, interest in X-ray diffraction imaging has taken flight and resulted in a wide variety of methods. This article discusses a new full-field imaging method, which uses polymer compound refractive lenses as a microscope objective to capture a diffracted X-ray beam coming from a large illuminated area on a sample. This produces an image of the diffracting parts of the sample on a camera. It is shown that this technique has added value in the field, owing to its high imaging speed, while being competitive in resolution and level of detail of obtained information. Using a model sample, it is shown that lattice tilts and strain in single crystals can be resolved simultaneously down to 10(-3o) and Delta a/a = 10(-5), respectively, with submicrometre resolution over an area of 100 x 100 mu m and a total image acquisition time of less than 60 s.
引用
收藏
页码:1882 / 1888
页数:7
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