Stress measurement using area detectors: a theoretical and experimental comparison of different methods in ferritic steel using a portable X-ray apparatus

被引:33
|
作者
Ramirez-Rico, J. [1 ]
Lee, S. -Y. [2 ]
Ling, J. J. [2 ]
Noyan, I. C. [2 ]
机构
[1] Univ Seville, CSIC, Fis Mat Condensada ICMS, E-41012 Seville, Spain
[2] Columbia Univ, Appl Phys & Appl Math, New York, NY 10027 USA
关键词
DIFFRACTION; GRADIENTS;
D O I
10.1007/s10853-016-9837-3
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
Using area detectors for stress determination by diffraction methods in a single exposure greatly simplifies the measurement process and permits the design of portable systems without complex sample cradles or moving parts. An additional advantage is the ability to see the entire or a large fraction of the Debye ring and thus determine texture and grain size effects before analysis. The two methods most commonly used to obtain stress from a single Debye ring are the so-called and full-ring fitting methods, which employ least-squares procedures to determine the stress from the distortion of a Debye ring by probing a set of scattering vector simultaneously. The widely applied method, in contrast, requires sample rotations to probe a different subset of scattering vector orientations. In this paper, we first present a description of the different methods under the same formalism and using a unified set of coordinates that are suited to area detectors normal to the incident beam, highlighting the similarities and differences between them. We further characterize these methods by means of in situ measurements in carbon steel tube samples, using a portable detector in reflection geometry. We show that, in the absence of plastic flow, the different methods yield basically the same results and are equivalent. An analysis of possible sources of errors and their impact in the final stress values is also presented.
引用
收藏
页码:5343 / 5355
页数:13
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