Synthesis and characterization of a new (E, E)-dioxime and its homo and heteronuclear complexes containing macrobicylic moieties

被引：11

作者：

Mendil, D ^{[1
]}

Bilgin, A ^{[1
]}

Gök, Y ^{[1
]}

Sentürk, HB ^{[1
]}

机构：

[1] Karadeniz Tech Univ, Dept Chem, TR-61080 Trabzon, Turkey

来源：

JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY | 2002年 / 43卷 / 3-4期

关键词：

BF2+-capped complex; cobalt(III) complex; diazatetraoxamacrobicycle; (E; E)-dioxime; heterotrinuclear complex; template effect;

D O I：

10.1023/A:1021279728967

中图分类号：

O6 [化学];

学科分类号：

0703 ;

摘要：

A new N,N'-substituted diaminoglyoxime (H2L) containing a diazatetraoxa macrobicycle [2.2.2(B)] has been synthesized from an aromatic primary amine attached to the cryptand moiety and cyanogen-di-N-oxide. The BF2+-capped Co(III) and heterotri-nuclear complexes of the vic-dioxime were prepared. The new compounds were characterized by a combination of elemental analysis and H-1 NMR, C-13 NMR, IR and MS spectral data.

引用

页码：265 / 270

页数：6

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