Synthesis and characterization of a new (E, E)-dioxime and its homo and heteronuclear complexes containing macrobicylic moieties

被引：11
|
作者：
Mendil, D [1 ]
Bilgin, A [1 ]
Gök, Y [1 ]
Sentürk, HB [1 ]
机构：
[1] Karadeniz Tech Univ, Dept Chem, TR-61080 Trabzon, Turkey
来源：
JOURNAL OF INCLUSION PHENOMENA AND MACROCYCLIC CHEMISTRY | 2002年 / 43卷 / 3-4期
关键词：
BF2+-capped complex; cobalt(III) complex; diazatetraoxamacrobicycle; (E; E)-dioxime; heterotrinuclear complex; template effect;
D O I：
10.1023/A:1021279728967
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
A new N,N'-substituted diaminoglyoxime (H2L) containing a diazatetraoxa macrobicycle [2.2.2(B)] has been synthesized from an aromatic primary amine attached to the cryptand moiety and cyanogen-di-N-oxide. The BF2+-capped Co(III) and heterotri-nuclear complexes of the vic-dioxime were prepared. The new compounds were characterized by a combination of elemental analysis and H-1 NMR, C-13 NMR, IR and MS spectral data.
引用
收藏
页码：265 / 270
页数：6
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