MoO3 Nanoparticles Synthesis via Hydro-Solvothermal Technique and Its Application as Catalyst for Efficient Ring Opening of Epoxides With Amines Under Solvent-Free Conditions

被引：9

作者：

Malakooti, Reihaneh ^{[1
]}

Shafie, Soheila ^{[1
]}

Hosseinabadi, Rahele ^{[1
]}

Heravi, Majid M. ^{[2
]}

Zakeri, Masoumeh ^{[2
]}

Mohammadi, Narges ^{[2
]}

机构：

[1] Univ Birjand, Dept Chem, Nanochem Res Lab, Birjand, Iran

[2] Alzahra Univ, Sch Sci, Dept Chem, Tehran, Iran

来源：

SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2014年 / 44卷 / 10期

关键词：

beta-aminoalcohol; metal oxide nanoparticles; molybdenum trioxide; solvent-free; AROMATIC-AMINES; MOLYBDENUM; NANOBELTS; ALCOHOLS; NANORODS; ANILINES; MILD; MORPHOLOGY; NANOWIRES; TRIFLATE;

D O I：

10.1080/15533174.2013.809740

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Molybdenum trioxide nanoparticles were synthesized using ammonium heptamolybdate tetrahydrate (AHM) through a facile hydro-solvothermal technique. The materials were characterized via X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The mean diameter of semispherical -MoO3 nanoparticles was determined to be 20 +/- 5nm. The catalytic performance of obtained products was examined in the ring opening of epoxides with diverse amines under solvent-free conditions in excellent yields and short period of times.

引用

页码：1401 / 1406

页数：6

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