MoO3 Nanoparticles Synthesis via Hydro-Solvothermal Technique and Its Application as Catalyst for Efficient Ring Opening of Epoxides With Amines Under Solvent-Free Conditions

被引：9
|
作者：
Malakooti, Reihaneh [1 ]
Shafie, Soheila [1 ]
Hosseinabadi, Rahele [1 ]
Heravi, Majid M. [2 ]
Zakeri, Masoumeh [2 ]
Mohammadi, Narges [2 ]
机构：
[1] Univ Birjand, Dept Chem, Nanochem Res Lab, Birjand, Iran
[2] Alzahra Univ, Sch Sci, Dept Chem, Tehran, Iran
来源：
SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2014年 / 44卷 / 10期
关键词：
beta-aminoalcohol; metal oxide nanoparticles; molybdenum trioxide; solvent-free; AROMATIC-AMINES; MOLYBDENUM; NANOBELTS; ALCOHOLS; NANORODS; ANILINES; MILD; MORPHOLOGY; NANOWIRES; TRIFLATE;
D O I：
10.1080/15533174.2013.809740
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Molybdenum trioxide nanoparticles were synthesized using ammonium heptamolybdate tetrahydrate (AHM) through a facile hydro-solvothermal technique. The materials were characterized via X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The mean diameter of semispherical -MoO3 nanoparticles was determined to be 20 +/- 5nm. The catalytic performance of obtained products was examined in the ring opening of epoxides with diverse amines under solvent-free conditions in excellent yields and short period of times.
引用
收藏
页码：1401 / 1406
页数：6
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