MoO3 Nanoparticles Synthesis via Hydro-Solvothermal Technique and Its Application as Catalyst for Efficient Ring Opening of Epoxides With Amines Under Solvent-Free Conditions

被引：9

作者：

Malakooti, Reihaneh ^{[1
]}

Shafie, Soheila ^{[1
]}

Hosseinabadi, Rahele ^{[1
]}

Heravi, Majid M. ^{[2
]}

Zakeri, Masoumeh ^{[2
]}

Mohammadi, Narges ^{[2
]}

机构：

[1] Univ Birjand, Dept Chem, Nanochem Res Lab, Birjand, Iran

[2] Alzahra Univ, Sch Sci, Dept Chem, Tehran, Iran

来源：

SYNTHESIS AND REACTIVITY IN INORGANIC METAL-ORGANIC AND NANO-METAL CHEMISTRY | 2014年 / 44卷 / 10期

关键词：

beta-aminoalcohol; metal oxide nanoparticles; molybdenum trioxide; solvent-free; AROMATIC-AMINES; MOLYBDENUM; NANOBELTS; ALCOHOLS; NANORODS; ANILINES; MILD; MORPHOLOGY; NANOWIRES; TRIFLATE;

D O I：

10.1080/15533174.2013.809740

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Molybdenum trioxide nanoparticles were synthesized using ammonium heptamolybdate tetrahydrate (AHM) through a facile hydro-solvothermal technique. The materials were characterized via X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The mean diameter of semispherical -MoO3 nanoparticles was determined to be 20 +/- 5nm. The catalytic performance of obtained products was examined in the ring opening of epoxides with diverse amines under solvent-free conditions in excellent yields and short period of times.

引用

页码：1401 / 1406

页数：6

共 50 条

[1] Calcium Trifluoroacetate as an Efficient Catalyst for Ring-opening of Epoxides by Amines under Solvent-free Conditions
Outouch, Rachid
Rauchdi, Mariem
Boualy, Brahim
El Firdoussi, Larbi
Roucoux, Alain
Ali, Mustapha Ait
ACTA CHIMICA SLOVENICA, 2014, 61 (01) : 67 - 72
[2] An efficient catalyst for ring opening of epoxides with phenol and thiophenol under solvent-free conditions
Lu, Hong-fei
Zhou, Jun-tao
Cheng, He-long
Sun, Lei-lei
Yang, Fei-fei
Wu, Run-ze
Gao, Yu-hua
Luo, Zhi-bin
TETRAHEDRON, 2013, 69 (52) : 11174 - 11184
[3] Efficient method for ring opening of epoxides with amines by NaY zeolite under solvent-free conditions
Kureshy, Rukhsana Ilyas
Singh, Surendra
Khan, Noor-ul Hasan
Abdi, Sayed Hasan Razi
Suresh, Eringathodi
Jasra, Raksh Vir
JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2007, 264 (1-2) : 162 - 169
[4] Scandium triflate as an efficient and useful catalyst for the synthesis of β-amino alcohols by regioselective ring opening of epoxides with amines under solvent-free conditions
Placzek, AT
Donelson, JL
Trivedi, R
Gibbs, RA
De, SK
TETRAHEDRON LETTERS, 2005, 46 (52) : 9029 - 9034
[5] Cyanuric chloride: an efficient catalyst for ring opening of epoxides with thiols under solvent-free conditions
Bandgar, Babasaheb P.
Joshi, Neeta S.
Kamble, Vinod T.
Sawant, Sanjay S.
AUSTRALIAN JOURNAL OF CHEMISTRY, 2008, 61 (03) : 231 - 234
[6] Sulfamic acid as an efficient and recyclable catalyst for the ring opening of epoxides with amines and anilines:: An easy synthesis of β-amino alcohols under solvent-free conditions
Kamal, Ahmed
Prasad, B. Rajendra
Reddy, A. Malla
Khan, M. Naseer A.
CATALYSIS COMMUNICATIONS, 2007, 8 (12) : 1876 - 1880
[7] Mg(ClO4)2, an Efficient Catalyst for Synthesis of -Amino Alcohols by Ring Opening of Epoxides with Amines under Solvent-Free Conditions
Jafari, Abbas Ali
Moradgholi
SYNTHETIC COMMUNICATIONS, 2011, 41 (04) : 594 - 602
[8] Sulfamic acid catalyzed ring opening of epoxides with amines under solvent-free conditions
M. Hosseini-Sarvari
H. Sharghi
Journal of the Iranian Chemical Society, 2008, 5 : 384 - 393
[9] Sulfamic acid catalyzed ring opening of epoxides with amines under solvent-free conditions
Hosseini-Sarvari, M.
Sharghi, H.
JOURNAL OF THE IRANIAN CHEMICAL SOCIETY, 2008, 5 (03) : 384 - 393
[10] Catalyst-free regioselective ring opening of epoxides with aromatic amines in water and solvent-free conditions
A. Ziyaei-Halimehjani
H. Gholami
M. R. Saidi
Journal of the Iranian Chemical Society, 2013, 10 : 7 - 11

← 1 2 3 4 5 →