Effect of Hydrochloric Acid Concentration on Morphology of Polyaniline Nanofibers Synthesized by Rapid Mixing Polymerization

被引:22
|
作者
Zakaria, Zulkhairi [1 ]
Halim, Nurul F. A. [1 ]
Schleusingen, Mubaraq H. V. [1 ]
Islam, A. K. M. Shafiqul [2 ]
Hashim, Uda [3 ]
Ahmad, Andmohd N. [1 ]
机构
[1] Univ Malaysia Perlis, Sch Mat Engn, Arau 02600, Perlis, Malaysia
[2] Univ Malaysia Perlis, Fac Engn Technol, Padang Besar 02100, Perlis, Malaysia
[3] Univ Malaysia Perlis, Inst Nano Elect Engn, Kangar 01000, Perlis, Malaysia
关键词
MECHANISMS; TEMPLATE;
D O I
10.1155/2015/218204
中图分类号
TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
Polyaniline (PANI) nanofibers with diameters ranging from 60 nm to 190 nm were successfully synthesized by rapid mixing polymerization method at room temperature. The effects of synthesis conditions such as concentration of hydrochloric acid (HCl), ammonium persulfate (APS), and aniline monomer (Ani) on the morphology of PANI nanofibers were investigated using scanning electron microscopy (SEM). FTIR and UV-Vis analysis were performed to characterize the PANI nanofibers. The effect of polymerization time and electrical properties of PANI nanofibers was also discussed. A rapid mixing polymerization method is found to be advantageous in producing bulk quantities of nanofibers.
引用
收藏
页数:6
相关论文
共 50 条
  • [31] The Effect of Solution Concentration and Deposition Time on Viscoelasticity and Morphology of Polyaniline Coating
    Rahayu, E. I. P.
    Putri, N. P.
    SEMINAR NASIONAL FISIKA (SNF) UNESA 2019, 2020, 1491
  • [32] Exploration on the microwave-assisted synthesis and formation mechanism of polyaniline nanostructures synthesized in different hydrochloric acid concentrations
    Qiu, Biwei
    Li, Zhoujing
    Wang, Xia
    Li, Xiaoyan
    Zhang, Jinrui
    JOURNAL OF POLYMER SCIENCE PART A-POLYMER CHEMISTRY, 2017, 55 (20) : 3357 - 3369
  • [33] Handedness switch of synthesized helical polyaniline nanofibers featuring the use of a single enantiomeric acid and aniline oligomers
    Li, Ruiqi
    Wang, Yudan
    Zhou, Dan
    Liu, Lijia
    Li, Junqing
    Li, Yufa
    Dai, Jijin
    Han, Yushan
    POLYMER, 2018, 159 : 39 - 46
  • [34] Sulfonated Polyaniline Nanostructures Synthesized via Rapid Initiated Copolymerization with Controllable Morphology, Size, and Electrical Properties
    Liao, Yaozu
    Strong, Veronica
    Chian, Wei
    Wang, Xia
    Li, Xin-Gui
    Kaner, Richard B.
    MACROMOLECULES, 2012, 45 (03) : 1570 - 1579
  • [35] Effect of low-concentration hydrochloric acid on properties of shale rocks
    1600, Society of Petroleum Engineers (SPE) (66):
  • [36] EFFECT OF CONCENTRATION UPON CHROMATOGRAPHIC BEHAVIOUR OF TECHNETIUM IN CONCENTRATED HYDROCHLORIC ACID
    WILLIAMS, MJ
    DEEGAN, T
    JOURNAL OF CHROMATOGRAPHY, 1971, 54 (01): : 123 - &
  • [37] Effect of the hydrochloric acid concentration on the hydrolysis of sorghum straw at atmospheric pressure
    Herrera, A
    Téllez-Luis, SJ
    González-Cabriales, JJ
    Ramírez, JA
    Vázquez, M
    JOURNAL OF FOOD ENGINEERING, 2004, 63 (01) : 103 - 109
  • [38] The effect of acetic acid on morphology of PZT nanofibers fabricated by electrospinning
    Hossain, Mynul
    Kim, Amkee
    MATERIALS LETTERS, 2009, 63 (9-10) : 789 - 792
  • [39] DEMONSTRATION OF A COCATALYTIC EFFECT OF WATER AND HYDROCHLORIC ACID ON POLYMERIZATION OF INDENE BY TIN TETRACHLORIDE
    POLTON, A
    SIGWALT, P
    COMPTES RENDUS HEBDOMADAIRES DES SEANCES DE L ACADEMIE DES SCIENCES SERIE C, 1967, 265 (23): : 1303 - &
  • [40] Effect of Sulfur Concentration on the Morphology of Carbon Nanofibers Produced from a Botanical Hydrocarbon
    Pradip Ghosh
    Tetsuo Soga
    Kaushik Ghosh
    Takashi Jimbo
    Ryoji Katoh
    Kenji Sumiyama
    Yoshinori Ando
    Nanoscale Research Letters, 3