Silica Sulfuric Acid as a Recyclable Catalyst for a One-Pot Synthesis of α-Aminophosphonates in Solvent-Free Conditions

被引:11
|
作者
Yang, Jing-Jun [1 ]
Dang, Ning [1 ]
Chang, Yu-Wei [1 ]
机构
[1] Gansu Normal Univ Nationalities, Dept Chem, Hezuo 747000, Gansu, Peoples R China
关键词
alpha-Aminophosphonates; aldehydes; amines; alkyl phosphite; three-component reaction; AMINO PHOSPHONATES; ANTIBACTERIAL AGENTS; HETEROGENEOUS SYSTEM; MILD CONDITIONS; 3-COMPONENT REACTION; LANTHANIDE TRIFLATE; BIOLOGICAL-ACTIVITY; REUSABLE CATALYST; PHOSPHONOPEPTIDES; EFFICIENT;
D O I
10.2174/157017809789124830
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
A simple and efficient method has been developed for the synthesis of alpha-aminophosphonates by a one-pot three-component condensation of aldehydes, amines and diethyl phosphite in the presence of a catalytic amount of silica sulfuric acid under solvent-free reaction conditions. The major advantages of the present method are good yields, inexpensive, ecofriendly and reusable catalyst, short reaction times, mild and solvent-free reaction conditions.
引用
收藏
页码:470 / 473
页数:4
相关论文
共 50 条
  • [41] Mandelic acid catalyzed one-pot three-component synthesis of α-aminonitriles and α-aminophosphonates under solvent-free conditions at room temperature
    Kaur, Gurpreet
    Shamim, Mussarat
    Bhardwaj, Vaishali
    Gupta, Vivek Kumar
    Banerjee, Bubun
    SYNTHETIC COMMUNICATIONS, 2020, 50 (10) : 1545 - 1560
  • [42] Sodium Dihydrogen Phosphate as an Efficient Catalyst for One-Pot, Three-Component Synthesis of -Aminophosphonates Under Solvent-Free Conditions at Room Temperature
    Karimi-Jaberi, Zahed
    Amiri, Mohammad
    Sadeghi, Naghmeh
    SYNTHETIC COMMUNICATIONS, 2010, 40 (19) : 2948 - 2953
  • [43] One-pot synthesis of xanthene derivatives under solvent-free conditions
    Dabiri, Minoo
    Azimi, Seyyedeh C.
    Bazgir, Ayoob
    CHEMICAL PAPERS, 2008, 62 (05): : 522 - 526
  • [44] Efficient One-Pot Synthesis of Benzimidazoles Under Solvent-Free Conditions
    Du, Li-Hua
    Luo, Xi-Ping
    SYNTHETIC COMMUNICATIONS, 2010, 40 (19) : 2880 - 2886
  • [45] One-pot synthesis of xanthene derivatives under solvent-free conditions
    Minoo Dabiri
    Seyyedeh C. Azimi
    Ayoob Bazgir
    Chemical Papers, 2008, 62 : 522 - 526
  • [46] One-Pot Synthesis of Mannich Bases Under Solvent-Free Conditions
    Demirkol, Onur
    Akbaslar, Dilek
    Giray, Sultan
    Anil, B. Baris
    SYNTHETIC COMMUNICATIONS, 2014, 44 (09) : 1279 - 1285
  • [47] TiO2 as a new and reusable catalyst for one-pot three-component syntheses of α-aminophosphonates in solvent-free conditions
    Hosseini-Sarvari, Mona
    TETRAHEDRON, 2008, 64 (23) : 5459 - 5466
  • [48] One-pot and three-component synthesis of substituted pyrimidines catalysed by boron sulfuric acid under solvent-free conditions
    Soheilizad, Mehdi
    Adib, Mehdi
    Sajjadifar, Sami
    JOURNAL OF CHEMICAL RESEARCH, 2014, (09) : 524 - 527
  • [49] One-pot synthesis of naphthopyranopyrimdine derivatives using nano silica phosphoric acid under thermal and solvent-free conditions
    Yaghmaeiyan, Nahid
    Mirzaei, Mahdi
    Bamoniri, Abdolhamid
    RESULTS IN CHEMISTRY, 2023, 5
  • [50] Facile one-pot synthesis of polysubstituted quinolines under solvent-free conditions using sulfamic acid as a reusable catalyst
    Min Zhang
    Biao Xiong
    Wei Yang
    D. N. T. Kumar
    Yu-Qiang Ding
    Monatshefte für Chemie - Chemical Monthly, 2012, 143 : 471 - 478