An improved synthesis of solid-supported reagents (SSRs) for selective acylation of amines by microwave irradiation

被引：26
|
作者：
Petricci, E [1 ]
Botta, M [1 ]
Corelli, F [1 ]
Mugnaini, C [1 ]
机构：
[1] Univ Studi Siena, Dipartimento Farm Chim Tecnol, I-53100 Siena, Italy
来源：
TETRAHEDRON LETTERS | 2002年 / 43卷 / 37期
关键词：
D O I：
10.1016/S0040-4039(02)01478-8
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
Microwave-assisted acylation of a solid-Supported pyrimidine linker with different acyl chlorides gave polymer-bound 4-acyloxypyrimidines, which in turn were used as SSRs for rapid and selective acylation of amines under microwave irradiation. (C) 2002 Elsevier Science Ltd. All rights reserved.
引用
收藏
页码：6507 / 6509
页数：3
相关论文
共 50 条
  • [31] Solid-Supported Odorless Reagents for the Dithioacetalization of Aldehydes and Ketones
    Jung, N.
    Graessle, S.
    Luetjohann, S.
    Braese, S.
    ORGANIC LETTERS, 2014, 16 (04) : 1036 - 1039
  • [32] Synthesis of nornicotine, nicotine and other functionalised derivatives using solid-supported reagents and scavengers
    Baxendale, IR
    Brusotti, G
    Matsuoka, M
    Ley, SV
    JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 2002, (02): : 143 - 154
  • [33] Convenient synthesis of 2,9-disubstituted guanines mediated by solid-supported reagents
    McComas, W
    Chen, L
    Kim, K
    TETRAHEDRON LETTERS, 2000, 41 (19) : 3573 - 3576
  • [34] Solid-supported synthesis of oligomeric bioconjugates
    Virta, P
    Katajisto, J
    Niittymäki, T
    Lönnberg, H
    TETRAHEDRON, 2003, 59 (28) : 5137 - 5174
  • [35] Chemoselective purification mediated by solid-supported reagents: The application to purine library synthesis.
    Kim, K
    McComas, W
    ABSTRACTS OF PAPERS OF THE AMERICAN CHEMICAL SOCIETY, 1999, 218 : U197 - U197
  • [36] Solid-Supported Synthesis of Artificial Phospholipids
    Furuta, Takumi
    Onuki, Hitoshi
    Mochizuki, Masayoshi
    Ito, Mai
    Inai, Makoto
    Wakimoto, Toshiyuki
    Kan, Toshiyuki
    SYNLETT, 2009, (20) : 3373 - 3377
  • [37] Combining the use of solid-supported transition metal catalysis with microwave irradiation in solution-phase parallel library synthesis
    Organ, Michael G.
    Mayer, Stanislas
    Lepifre, Franck
    N'Zemba, Blaise
    Khatri, Jayantilal
    MOLECULAR DIVERSITY, 2003, 7 (2-4) : 211 - 227
  • [38] Microwave-assisted synthesis utilizing supported reagents: A rapid and efficient acylation procedure
    Sauer, DR
    Kalvin, D
    Phelan, KM
    ORGANIC LETTERS, 2003, 5 (24) : 4721 - 4724
  • [39] Solid-supported reagents and catalysts for the preparation of large ring compounds
    Elisabeth Gonthier
    Rolf Breinbauer
    Molecular Diversity, 2005, 9 : 51 - 62
  • [40] Solid-supported reagents and catalysts for the preparation of large ring compounds
    Gonthier, Elisabeth
    Breinbauer, Rolf
    MOLECULAR DIVERSITY, 2005, 9 (1-3) : 51 - 62
12345