1,1′,2,2′-Tetramethyl-3,3′-(4-methoxybenzylidene)di-1H-indole

被引:0
|
作者
Zhang, Cai-Li [1 ]
Ye, Ping-Ping [1 ]
Du, Zhi-Qiang [1 ]
机构
[1] Zhejiang Univ, Dept Chem, Hangzhou 310027, Zhejiang, Peoples R China
基金
中国国家自然科学基金;
关键词
D O I
10.1107/S1600536809017759
中图分类号
O7 [晶体学];
学科分类号
0702 ; 070205 ; 0703 ; 080501 ;
摘要
The title compound, C28H28N2O, was prepared by condensation of 1,2-bimethylindole and 4-methoxybenzaldehyde. In the molecular structure, the plane of the non-fused benzene ring is twisted with respect to the planes of the two indole ring systems, exhibiting dihedral angles of 72.04 (7) and 72.24 (7)degrees, while the planes of the two indole ring systems are oriented at a dihedral angle of 87.05 (5)degrees. Neither hydrogen bonding nor pi-pi stacking is observed in the crystal structure.
引用
收藏
页码:O1332 / U2323
页数:9
相关论文
共 50 条
  • [41] (S)-2,2′-bis(methoxymethoxy)[1,1′-binaphthyl]-3,3′- dicarbaldehyde
    Tachi, Y
    Nakayama, S
    Tani, F
    Ueno, G
    Naruta, Y
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1999, 55 : 1351 - 1353
  • [42] 2,2",3,3",4,4",5,5"-Octaphenyl-1,1′:4′,1"-terphenyl and 2′,3′,5′,6′-tetrafluoro-2,2",3,3",4,4",5,5"-octaphenyl-1,1′:4′,1"-terphenyl
    Budy, Stephen M.
    Nichol, Gary S.
    Loy, Douglas A.
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2012, 68 : O23 - O27
  • [43] 2-dipentylamino-4-(4-methoxybenzylidene)-1-phenyl-1H-imidazol-5(4H)-one
    Ma, Rui
    Song, Zhong-Ying
    Liu, Yan
    Bai, Yi-Qiong
    Bao, Feng
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2007, 63 : O3336 - U4621
  • [44] 1:1 adduct of 1,1′-bis(dibromoboryl)ferrocene and 3,3′,4,4′-tetramethyl-1,1′-diphosphaferrocene
    Scheibitz, M
    Bolte, M
    Lerner, HW
    Wagner, M
    ORGANOMETALLICS, 2004, 23 (14) : 3556 - 3559
  • [45] NOVEL CONVENIENT SYNTHESIS OF 2,2',6,6'-TETRAMETHYL-3,3'-AZOPYRIDINE
    PUSZYNSKI, A
    RYKOWSKI, Z
    ROCZNIKI CHEMII, 1977, 51 (12): : 2451 - 2453
  • [46] 1,1′,5,5′-Tetramethyl-2,2′-diphenyl-4,4′-[p-phenylenebis(methylidynenitrilo)]di-1H-pyrazol-3(2H)-one
    Xiao, Yan
    Bi, Cai Feng
    Wang, Ai Dong
    Fan, Yu Hua
    Zhang, Xia
    Xu, Jia Kun
    Xie, Si Tang
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O1479 - U2174
  • [47] Crystal structures of 2 '-benzoyl-1 '-(4-methylphenyl)-1,1 ',2,2 ',5 ',6 ',7 ',7a '-octahydrospiro [indole3,3 '-pyrrolizin]-2-one and 2 '-(4-bromobenzoyl)-1 '(2-chlorophenyl)-1,1 ',2,2 ',5 ',6 ',7 ',7a '-octahydrospiro [indole-3,3 '-pyrrolizin]-2-one
    Chandrarekha, M.
    Srinivasan, N.
    Vijaya, P. Kottala
    Siva, A.
    Krishnakumar, R. V.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2016, 72 : 1637 - +
  • [48] 1,1′-Dibutyl-3,3′-biindolinylidene-2,2′-dione
    Yuan, Mao-Sen
    Fang, Qi
    Ji, Lei
    Yu, Wen-Tao
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : O4342 - U3617
  • [49] 1,1′,3,3′-tetramethyl-2,2′-diimidazolium dication:: Its bromide salt and the tetraphenylborates of its ketone adducts
    Nagel, N
    Bock, H
    Eller, P
    ZEITSCHRIFT FUR KRISTALLOGRAPHIE, 2000, 215 (01): : 39 - 44
  • [50] PHOTOCYCLIZATION OF 3,3'-DIPHENYL-2,2'-BI-1H-INDENE-1,1'-DIONE
    TODA, F
    TODO, Y
    BULLETIN OF THE CHEMICAL SOCIETY OF JAPAN, 1977, 50 (11) : 3000 - 3001