1,1′,2,2′-Tetramethyl-3,3′-(4-methoxybenzylidene)di-1H-indole

被引：0
|
作者：
Zhang, Cai-Li [1 ]
Ye, Ping-Ping [1 ]
Du, Zhi-Qiang [1 ]
机构：
[1] Zhejiang Univ, Dept Chem, Hangzhou 310027, Zhejiang, Peoples R China
来源：
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2009年 / 65卷
基金：
中国国家自然科学基金;
关键词：
D O I：
10.1107/S1600536809017759
中图分类号：
O7 [晶体学];
学科分类号：
0702 ; 070205 ; 0703 ; 080501 ;
摘要：
The title compound, C28H28N2O, was prepared by condensation of 1,2-bimethylindole and 4-methoxybenzaldehyde. In the molecular structure, the plane of the non-fused benzene ring is twisted with respect to the planes of the two indole ring systems, exhibiting dihedral angles of 72.04 (7) and 72.24 (7)degrees, while the planes of the two indole ring systems are oriented at a dihedral angle of 87.05 (5)degrees. Neither hydrogen bonding nor pi-pi stacking is observed in the crystal structure.
引用
收藏
页码：O1332 / U2323
页数：9
相关论文
共 50 条
  • [31] Crystal structures of 1,1′-di(methylacetato)- and 1,1′-di(chloroethoxyethyl)-2,2′-biimidazole
    W. Mark Barnett
    Geng Lin
    Harvest L. Collier
    Russell G. Baughman
    Journal of Chemical Crystallography, 1997, 27 (7) : 423 - 427
  • [32] 4-Isopropyl-2-(4-methoxybenzylidene)3,4-dihydronaphthalen-1(2H)-one
    Al Houari, G
    Kerbal, A
    El Bali, B
    Bolte, M
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O3330 - O3331
  • [33] Synthesis and structure determination of stereoisomeric 2,2'-dibenzoyl-3,3', 4,4'-tetramethyl-1,1'-diphosphaferrocenes
    Klys, Arkadiusz
    Malecka, Magdalena
    Zakrzewski, Janusz
    ARKIVOC, 2007, : 172 - 178
  • [34] Resolution and determination of the absolute configuration 2,2′-diacetyl-3,3′, 4,4′-tetramethyl-1,1′-diphosphaferrocenes
    Klys, Arkadiusz
    JOURNAL OF ORGANOMETALLIC CHEMISTRY, 2012, 700 : 1 - 3
  • [35] BIMOLECULAR REDUCTION OF ISOQUINOLINE - EPIMERIC 1,1',2,2',3,3',4,4'-OCTAHYDRO-1,1'-BIISOQUINOLINES AND DERIVATIVES
    NIELSEN, AT
    JOURNAL OF ORGANIC CHEMISTRY, 1970, 35 (08): : 2498 - &
  • [36] (Z)-3-(4-methoxybenzylidene)-2-methylisoindolin-1-one
    Warzecha, KD
    Neudörfl, JM
    Griesbeck, AG
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O1074 - O1075
  • [37] [μ-1,1′-Bis(2,4,6-trimethylbenzyl)-3,3′-(2,3,5,6-tetramethyl-p-phenylenedibenzimidazole)-2,2′-diylidene]di-μ-bromo-disilver(I)
    Kosar, Basak
    Turkmen, Hayati
    Cetinkaya, Bekir
    Buyukgungor, Orhan
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2007, 63 : M619 - M620
  • [38] (E)-1-(4-Methoxybenzylidene)-2-phenylhydrazine
    Mufakkar, Muhammad
    Tahir, M. Nawaz
    Tariq, Muhammad Ilyas
    Ahmad, Shahbaz
    Sarfraz, Muhammad
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : O1887 - U62
  • [39] Reaction of 2,2′-Di(4-chlorophenyl)-1,1′,3,3′-tetraoxo-2,2′,3,3′-tetrahydro-1H,1′H-6,6′-di(benzo[de]isoquinoline)-7,7′-dicarboxylic Acid with Thiourea Dioxide in Water-Alkaline Solution
    Yu. V. Polenov
    K. S. Nikitin
    E. V. Egorova
    D. A. Patrusheva
    Russian Journal of General Chemistry, 2021, 91 : 631 - 635
  • [40] Reaction of 2,2′-Di(4-chlorophenyl)-1,1′,3,3′-tetraoxo-2,2′,3,3′-tetrahydro-1H,1′H-6,6′-di(benzo[de]isoquinoline)-7,7′-dicarboxylic Acid with Thiourea Dioxide in Water-Alkaline Solution
    Polenov, Yu. V.
    Nikitin, K. S.
    Egorova, E. V.
    Patrusheva, D. A.
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2021, 91 (04) : 631 - 635
12345