AN EFFICIENT GREEN SYNTHESIS OF NOVEL α-DIAMINOPHOSPHONATES

被引：5

作者：

Sampath, C. ^{[1
]}

Harika, P. ^{[2
]}

机构：

[1] Univ Zululand, Dept Chem, ZA-3886 Kwa Dlangezwa, Kwazulu Natal, South Africa

[2] Andhra Loyola Inst Engn & Technol, Dept Chem, Vijayawada, Andhra Pradesh, India

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2015年 / 190卷 / 11期

基金：

新加坡国家研究基金会;

关键词：

alpha-Diaminophosphonates; green synthesis; Kabachnik-Fields reaction; AMINO PHOSPHONATES; ACID; INHIBITORS; CHLORIDE; ANALOGS;

D O I：

10.1080/10426507.2015.1031756

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

A simple, novel, efficient, and environmentally benign protocol has been established for the synthesis of -diaminophosphonates in good to excellent yields (74-93%) by a one-pot, three-component reaction of 4,4-dioxyaniline, various aryl/heteroaryl aldehydes, and diphenyl H-phosphonate by using polyethylene glycol (PEG-600) in water as a green solvent at 80 degrees C via Kabachnik-Fields reaction. The structures of all newly synthesized compounds were characterized by IR, H-1, C-13, P-31 NMR, mass spectrometry, and elemental analysis.

引用

页码：1893 / 1900

页数：8

共 50 条

[31] Synthesis of Novel Nanocellulose Aerogel Supported Pd Complex: Green and Efficient Catalyst for Heck Coupling Reaction
Moujahid, Ouafa
Kassem, Ihsane
Ben Hamou, Karima
El Adlaoui, Sarnia
Kaddami, Hamid
Belachemi, Larbi
PROCEEDINGS OF 2017 INTERNATIONAL RENEWABLE & SUSTAINABLE ENERGY CONFERENCE (IRSEC' 17), 2017, : 509 - 512
[32] A novel green approach for the synthesis of tungsten oxide nanorods and its efficient potential towards photocatalytic degradation of reactive green 19 dye
Jagpreet Singh
Harjot Kaur
Mohit Rawat
Journal of Materials Science: Materials in Electronics, 2018, 29 : 13715 - 13722
[33] A novel green approach for the synthesis of tungsten oxide nanorods and its efficient potential towards photocatalytic degradation of reactive green 19 dye
Singh, Jagpreet
Kaur, Harjot
Rawat, Mohit
JOURNAL OF MATERIALS SCIENCE-MATERIALS IN ELECTRONICS, 2018, 29 (16) : 13715 - 13722
[34] An efficient catalytic synthesis of flavanones under green conditions
Jiang, Heyan
Zheng, Xuxu
Yin, Zhongyi
Xie, Jingjing
JOURNAL OF CHEMICAL RESEARCH, 2011, (04) : 220 - 221
[35] Efficient Industrial Organic Synthesis and the Principles of Green Chemistry
Schaub, Thomas
CHEMISTRY-A EUROPEAN JOURNAL, 2021, 27 (06) : 1865 - 1869
[36] Green synthesis of adsorbent nanoflowers for efficient removal of toxins
Nikita P. Devlekar
Pravin Shende
Chemical Papers, 2022, 76 : 2209 - 2219
[37] An efficient and green method for the synthesis of oxindole derivatives in water
Srihari, G.
Murthy, M. Marthanda
CHEMISTRY LETTERS, 2008, 37 (03) : 268 - 269
[38] Green and efficient synthesis route of catechol from guaiacol
Yang, Le
Zhou, Wei
Seshan, K.
Li, Yongdan
JOURNAL OF MOLECULAR CATALYSIS A-CHEMICAL, 2013, 368 : 61 - 65
[39] The efficient synthesis of carbon dots with green and blue fluorescence
Sun, Yuqing
Liu, Qi
Guo, Xiao
Guo, Mengxue
Han, Cuiping
BASIC & CLINICAL PHARMACOLOGY & TOXICOLOGY, 2019, 125 : 230 - 231
[40] Efficient green synthesis of α-aminonitriles, precursors of α-amino acids
Prakash, G. K. Surya
Thomas, Tisa Elizabeth
Bychinskaya, Inessa
Prakash, Arjun G.
Panja, Chiradeep
Vaghoo, Habiba
Olah, George A.
GREEN CHEMISTRY, 2008, 10 (10) : 1105 - 1110

← 1 2 3 4 5 →