Synthesis of new series of 1,8-bis (4-amino-5-mercapto 1,2,4-triazol-3-yl) octanes and their derivatives

被引：0
|
作者：
Kudari, SM [1 ]
Badiger, SE [1 ]
机构：
[1] Gulbarga Univ, Dept Chem, Gulbarga 585106, India
来源：
INDIAN JOURNAL OF HETEROCYCLIC CHEMISTRY | 1999年 / 9卷 / 02期
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D O I：
暂无
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
1,8-Bis (4-amino 5-mercapto-1,2,4-triazol-3-yl) octane (1) on reacting with hydrazine hydrate/chloroacetic acid and sodium acetate/benzoin and alcoholic potassium hydroxide/various substituted benzoic acids and phosphorous oxy chloride/isothiocyanates and EDAC afforded 1,8-bis (4-amino 5-hydrazino-1,2,4-triazol-3-yl) octane (II), 1,8-bis (1,2,4-triazol [4,5-b] thiadiazine 6[7H] one 3-yl) octane (III), 1,8- bis (1,2,4-triazol [4,5-b] thiadiazol-6-[5H] thion-3-yl) octane (V), 1,8-bis (1,2,4-triazol 6-aryl substituted [4,5-b]-1,3,4-thiadiazol-3-yl) octanes (Vla-f) and 1,8-bis (6-arylamino 1,2,4-triazol [4,5-b] 1,3,4-thiadiazol-3-yl) octanes (Vlla-b) respectively. The structure of the newly synthesized compounds have been characterized by IR, NMR 'and elemental analysis.
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页码：99 / 102
页数：4
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