Synthesis of new series of 1,8-bis (4-amino-5-mercapto 1,2,4-triazol-3-yl) octanes and their derivatives

被引:0
|
作者
Kudari, SM [1 ]
Badiger, SE [1 ]
机构
[1] Gulbarga Univ, Dept Chem, Gulbarga 585106, India
关键词
D O I
暂无
中图分类号
O62 [有机化学];
学科分类号
070303 ; 081704 ;
摘要
1,8-Bis (4-amino 5-mercapto-1,2,4-triazol-3-yl) octane (1) on reacting with hydrazine hydrate/chloroacetic acid and sodium acetate/benzoin and alcoholic potassium hydroxide/various substituted benzoic acids and phosphorous oxy chloride/isothiocyanates and EDAC afforded 1,8-bis (4-amino 5-hydrazino-1,2,4-triazol-3-yl) octane (II), 1,8-bis (1,2,4-triazol [4,5-b] thiadiazine 6[7H] one 3-yl) octane (III), 1,8- bis (1,2,4-triazol [4,5-b] thiadiazol-6-[5H] thion-3-yl) octane (V), 1,8-bis (1,2,4-triazol 6-aryl substituted [4,5-b]-1,3,4-thiadiazol-3-yl) octanes (Vla-f) and 1,8-bis (6-arylamino 1,2,4-triazol [4,5-b] 1,3,4-thiadiazol-3-yl) octanes (Vlla-b) respectively. The structure of the newly synthesized compounds have been characterized by IR, NMR 'and elemental analysis.
引用
收藏
页码:99 / 102
页数:4
相关论文
共 50 条
  • [31] Synthesis of new series of 1,8-bis-(4-aryl amino methyl 1,3,4-oxadiazolyl-5-thion-2-yl) octanes, 1,8-bis-(5-thio acetic/formic acid hydrazide/acetic acid 1,3,4-oxadiazol-2-yl) octanes
    Kudari, SM
    Badiger, SE
    ASIAN JOURNAL OF CHEMISTRY, 1998, 10 (03) : 462 - 466
  • [32] Microwave-assisted synthesis of double-headed derivatives of (4-amino-5-mercapto-4H-1,2,4-triazol-3-yl)-ethan-1-ol and study of their biological activity
    Reda A. Haggam
    Research on Chemical Intermediates, 2021, 47 : 3733 - 3749
  • [33] Microwave-assisted synthesis of double-headed derivatives of (4-amino-5-mercapto-4H-1,2,4-triazol-3-yl)-ethan-1-ol and study of their biological activity
    Haggam, Reda A.
    RESEARCH ON CHEMICAL INTERMEDIATES, 2021, 47 (09) : 3733 - 3749
  • [34] A novel mild method for the synthesis of 3-amino-4-(5-aryl-1H-1,2,4-triazol-3-yl)furazans
    Semyakin, Svyatoslav S.
    Struchkova, Marina I.
    Sheremetev, Aleksei B.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2016, 52 (05) : 346 - 349
  • [35] A Novel Mild Method for the Synthesis of 3-Amino-4-(5-aryl-1H-1,2,4-Triazol-3-yl)Furazans
    Svyatoslav S. Semyakin
    Marina I. Struchkova
    Aleksei B. Sheremetev
    Chemistry of Heterocyclic Compounds, 2016, 52 : 346 - 349
  • [36] Coordination compounds of copper(II) with bis(5-amino-1,2,4-triazol-3-yl)alkanes
    Barmin, MI
    Chekrenev, SA
    Kartavykh, VP
    Mel'nikov, VV
    RUSSIAN JOURNAL OF GENERAL CHEMISTRY, 2003, 73 (03) : 482 - 487
  • [37] KINETICS OF THERMAL DECOMPOSITION OF BIS(4-AMINO-5-MERCAPTO-1,2,4-TRIAZOL-3-YL)METHANE (BAMTM) UNDER NON-ISOTHERMAL CONDITION
    Manikandan, G.
    Jayabharathi, J.
    Rajarajan, G.
    Thanikachalam, V.
    OXIDATION COMMUNICATIONS, 2011, 34 (03): : 684 - 700
  • [38] Studies on some N-bridged heterocycles derived from bis-[4-amino-5-mercapto-1,2,4-triazol-3-yl] alkanes
    Holla, BS
    Gonsalves, R
    Shenoy, S
    FARMACO, 1998, 53 (8-9): : 574 - 578
  • [39] An effective synthesis of (1De-1,2,4-triazol-3-yl)furoxans
    Fershtat, Leonid L.
    Epishina, Margarita A.
    Ovchinnikov, Igor V.
    Kachala, Vadim V.
    Makhova, Nina N.
    CHEMISTRY OF HETEROCYCLIC COMPOUNDS, 2015, 51 (08) : 754 - 759
  • [40] 1,4-Bis(5-methyl-1H-1,2,4-triazol-3-yl)benzene tetrahydrate
    Zhu, Ai-Xin
    Chen, Xiu-Li
    Li, Zhen
    Du, Yuan-Chao
    Wang, Hong-Can
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1255 - U1612