(3R*,3′R*)-1,1′-Dimethyl-3,3′-biindoline-2,2′-dithione

被引:3
|
作者
Baumeister, U [1 ]
Hartung, H
Spitzner, R
Felicetti, M
Schroth, W
机构
[1] Univ Halle Wittenberg, Inst Phys Chem, D-06099 Halle, Germany
[2] Univ Halle Wittenberg, Inst Organ Chem, D-06099 Halle, Germany
关键词
D O I
10.1107/S0108270100004194
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The (3R*,3' R*) configuration of the title compound, C18H16- N2S2, (I), has been unambiguously elucidated by X-ray analysis. Molecules of (I) have C-2 symmetry to a good approximation and a strongly folded shape. The interplanar angle between the two halves of a molecule is 67.11 (6)degrees.
引用
收藏
页码:830 / 831
页数:2
相关论文
共 50 条
  • [41] 1,1',2,2'-TETRATHIAFULVALENES .3. SYNTHESIS, PROPERTIES, AND REACTIONS OF 3,3'-BI(3H-1,2-DITHIOLYLIDENES) (1,1',2,2'-TETRATHIAFULVALENES)
    BEHRINGER, H
    MEINETSBERGER, E
    LIEBIGS ANNALEN DER CHEMIE, 1981, (11): : 1928 - 1959
  • [42] cis-(3R,5R)-3-Bromo-2,2-dimethyl-5-phenyltetrahydropyran
    Hartung, J
    Svoboda, I
    Schmidt, P
    Pfeiffer, M
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2005, 61 : O15 - O16
  • [43] Diastereoselective synthesis of (2S*,3R*)- and (2R*,3R*)-2,6-dimethyl-2-homoprenyl-chroman-3-ol
    Inoue, S
    Asami, M
    Honda, K
    Shrestha, KS
    Takahashi, M
    Yoshino, T
    SYNLETT, 1998, (06) : 679 - +
  • [44] An efficient conversion of (3R,3′R,6′R)-lutein to (3R,3′S,6′R)-lutein (3′-epilutein) and (3R,3′R)-zeaxanthin
    Khachik, F
    JOURNAL OF NATURAL PRODUCTS, 2003, 66 (01): : 67 - 72
  • [45] 3,3′-dimethyl-1,1′-methylenediimidazolium tetrachlorocobaltate(II)
    Zeller, A
    Herdtweck, E
    Strassner, T
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2005, 61 (01): : M46 - M47
  • [46] SYNTHESIS OF 3,3'-DIMETHYL-1,1'-AZOBENZIMIDAZOLIUM SALTS
    GLOVER, EE
    ROWBOTTO.KT
    JOURNAL OF THE CHEMICAL SOCIETY-PERKIN TRANSACTIONS 1, 1973, (08): : 842 - 845
  • [47] 2,2′-Bis(methoxymethoxy)-3,3′-diphenyl-1,1′-binaphthalene
    Zong, Hua
    Huang, Hua-Yin
    Hu, Bing
    Bian, Guang-Ling
    Song, Ling
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O222 - U3316
  • [48] (R)-3,3'-二羧酸-1,1'-联萘酚的合成
    蒋胜前
    王周玉
    蒋珍菊
    李建惠
    西华大学学报(自然科学版), 2011, (02) : 99 - 101
  • [49] 3,3′-(2,2′-Bi-1H-imidazole-1,1′-diyl)dipropanamide
    Zhi, Y. -X.
    Long, J.
    Chen, J. -Y.
    Ren, Y. -T.
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O2008 - U4277
  • [50] 3,3′-(2,2′-Bi-1H-imidazole-1,1′-diyl)dipropanol
    Zhang, Tao
    Liang, Hong-Ze
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O213 - U1159