(3R*,3′R*)-1,1′-Dimethyl-3,3′-biindoline-2,2′-dithione

被引:3
|
作者
Baumeister, U [1 ]
Hartung, H
Spitzner, R
Felicetti, M
Schroth, W
机构
[1] Univ Halle Wittenberg, Inst Phys Chem, D-06099 Halle, Germany
[2] Univ Halle Wittenberg, Inst Organ Chem, D-06099 Halle, Germany
关键词
D O I
10.1107/S0108270100004194
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
The (3R*,3' R*) configuration of the title compound, C18H16- N2S2, (I), has been unambiguously elucidated by X-ray analysis. Molecules of (I) have C-2 symmetry to a good approximation and a strongly folded shape. The interplanar angle between the two halves of a molecule is 67.11 (6)degrees.
引用
收藏
页码:830 / 831
页数:2
相关论文
共 50 条
  • [21] Synthesis of (1R,3R)-3-[2-(aminoethyl)-2,2-dimethylcyclobutyl]methanol and (1S,3R)-(3-amino-2,2-dimethylcyclobutyl)methanol from (+)-nopinone
    Figueira, MJ
    Blanco, JM
    Caamaño, O
    Fernández, F
    García-Mera, X
    López, C
    SYNTHESIS-STUTTGART, 2000, (10): : 1459 - 1463
  • [22] 3R, 1R or 3R+1R? The Teachers' Dilemma
    Liu, Ong Puay
    Ting, Helen
    Tee, Ong Puay
    Hoon, Ong Puay
    INTERNATIONAL CONFERENCE ON LEARNER DIVERSITY 2010, 2010, 7 : 191 - 200
  • [23] 3,3"-Dimethyl-1,1′:4′,1"-terphenyl
    Avery, TD
    Taylor, DK
    Tiekink, ERT
    ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS, 1998, 54 : 148 - 149
  • [24] 3,3″-Dimethyl-1,1′:4′,1″-terphenyl
    Avery, Tom D.
    Taylor, Dennis K.
    Tiekink, Edward R.T.
    Acta Crystallographica, Section C: Crystal Structure Communications, 1998, 54 (pt 1): : 148 - 149
  • [25] 2,2′-Dimethyl-3,3′-bis(methylsulfanyl)-5,5′-bis(1-benzofuran)
    Choi, HD
    Kang, BW
    Seo, PJ
    Son, BW
    Lee, U
    ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2006, 62 : O2092 - O2094
  • [26] Methyl (3R*,3 ' S*)-1 ',1"-dimethyl-2,2"dioxodispiro[indoline-3,2 '-pyrrolidine-3 ',3"-indoline]-4 '-carboxylate
    Ganesh, G.
    Yuvaraj, Panneer Selvam
    Govindan, E.
    Reddy, Boreddy S. R.
    SubbiahPandi, A.
    ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : O2902 - +
  • [27] Synthesis and configuration of (1S,3R)- and (1R,3R)-1-(3,4-dimethoxyphenyl)-1,3-dimethyl-1,3-dihydroisobenzofurans
    Shishkina, Irina N.
    Demyanovich, Valeriya M.
    Potekhin, Konstantin A.
    Gurbanov, Atash V.
    Zefirov, Nikolay S.
    MENDELEEV COMMUNICATIONS, 2015, 25 (01) : 11 - 12
  • [28] Radical anions and dianions of 3,3′-bi(2-R-5,5-dimethyl-4-oxopyrrolinylidene) 1,1′-dioxides
    Shundrin, LA
    Reznikov, VA
    Irtegova, IG
    Starichenko, VF
    RUSSIAN CHEMICAL BULLETIN, 2003, 52 (04) : 939 - 943
  • [29] Radical anions and dianions of 3,3"-bi(2-R-5,5-dimethyl-4-oxopyrrolinylidene) 1,1"-dioxides
    L. A. Shundrin
    V. A. Reznikov
    I. G. Irtegova
    V. F. Starichenko
    Russian Chemical Bulletin, 2003, 52 : 939 - 943
  • [30] 1,1′-diacetyl-3-hydroxy-2,2′,3,3′-tetrahydro-3,3′-bi(1H-indole)-2,2′-dione
    Usman, A
    Razak, IA
    Fun, HK
    Chantrapromma, S
    Zhao, BG
    Xu, JH
    ACTA CRYSTALLOGRAPHICA SECTION C-STRUCTURAL CHEMISTRY, 2002, 58 (01): : O24 - O25