N,N'-dibromo-N,N'-1,2-ethanediylbis (benzene sulfonamide) as a novel N-Bromo Reagent-catalyzed trimethylsilylation of alcohols and phenol with hexamethyldisilazane in both solution and solvent-free conditions

被引：10

作者：

Khazaei, Ardeshir

Rostami, Amin

Rahmati, Sadegh

Mahboubifar, Marjan

机构：

[1] Bu Ali Sina Univ, Fac Sci, Dept Chem, Hamadan, Iran

[2] Kurdistan Univ, Dept Chem, Sanandaj, Iran

来源：

PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2007年 / 182卷 / 03期

关键词：

alcohols; phenols; N',N'-dibromo-N,N'-1,2-ethanediylbis (benzene sulfonamide); hexamethyldisilazane; trimethylsilylation; solvent-free;

D O I：

10.1080/10426500601013232

中图分类号：

O61 [无机化学];

学科分类号：

070301 ; 081704 ;

摘要：

Preparation and catalytic application of N,N'-dibromo-N,N'-1,2-ethanediylbis (benzene sulfonamide) for the trimethylsilylation of several of alcohols and phenols with hexamethyldisilazane in good to excellent yields under both solution and solvent-free conditions at r.t. is descried.

引用

页码：537 / 544

页数：8

共 45 条

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