N,N'-dibromo-N,N'-1,2-ethanediylbis (benzene sulfonamide) as a novel N-Bromo Reagent-catalyzed trimethylsilylation of alcohols and phenol with hexamethyldisilazane in both solution and solvent-free conditions

被引：10
|
作者：
Khazaei, Ardeshir
Rostami, Amin
Rahmati, Sadegh
Mahboubifar, Marjan
机构：
[1] Bu Ali Sina Univ, Fac Sci, Dept Chem, Hamadan, Iran
[2] Kurdistan Univ, Dept Chem, Sanandaj, Iran
来源：
PHOSPHORUS SULFUR AND SILICON AND THE RELATED ELEMENTS | 2007年 / 182卷 / 03期
关键词：
alcohols; phenols; N',N'-dibromo-N,N'-1,2-ethanediylbis (benzene sulfonamide); hexamethyldisilazane; trimethylsilylation; solvent-free;
D O I：
10.1080/10426500601013232
中图分类号：
O61 [无机化学];
学科分类号：
070301 ; 081704 ;
摘要：
Preparation and catalytic application of N,N'-dibromo-N,N'-1,2-ethanediylbis (benzene sulfonamide) for the trimethylsilylation of several of alcohols and phenols with hexamethyldisilazane in good to excellent yields under both solution and solvent-free conditions at r.t. is descried.
引用
收藏
页码：537 / 544
页数：8
相关论文
共 45 条
  • [21] Solvent-free oxidative deprotection of 1,3-dithianes and 1,3-dithiolanes using poly(N,N′-dibromo-N-ethyl-benzene-1,3-disulfonamide), N,N,N′,N′-tetrabromobenzene-1,3-disulfonamide and NBS
    Ghorbani-Vaghei, Ramin
    Veisi, Hojat
    ARKIVOC, 2009, : 44 - 51
  • [22] Solvent-free Synthesis of 1,8-Dioxo-octahydroxanthenes and Tetra-hydrobenzo[a]xanthene-11-ones over Poly(N,N-dibromo-N-ethylnaphtyl-2,7-sulfonamide)
    Khazaei, Ardeshir
    Rezaei, Mahshid
    Moosavi-Zare, Ahmad Reza
    Saednia, Shahnaz
    JOURNAL OF THE CHINESE CHEMICAL SOCIETY, 2017, 64 (09) : 1088 - 1095
  • [23] Selective conversion of alcohols and phenols to tetrahydropyranyl ethers catalyzed with N-chlorosaccharin under mild and solvent-free conditions
    Aghapour, Ghasem
    Moghaddam, Ali Kazemi
    Nadali, Samaneh
    IRANIAN JOURNAL OF CATALYSIS, 2016, 6 (05): : 455 - 459
  • [24] N,N,N′,N′-Tetrabromobenzene-1,3-disulfonamide and Poly(N-bromo-N-ethylbenzene-1,3-disulfonamide) as Mild and Efficient Catalysts for Solvent-free Synthesis of N-Cyclohexyl-2-aryl(alkyl)-imidazo[1,2-a]pyridin-3-amine Derivatives
    Ghorbani-Vaghei, Ramin
    Amiri, Mostafa
    JOURNAL OF HETEROCYCLIC CHEMISTRY, 2014, 51 : E372 - E379
  • [25] Novel and efficient protocol for the syntheses of N-1 substituted thiohydantoin and a bicyclothiohydantoin under solvent-free conditions
    Kumar, Vinod
    Rana, Hemlata
    Sankolli, Ravish
    Kaushik, M. P.
    TETRAHEDRON LETTERS, 2012, 53 (19) : 2377 - 2379
  • [26] Synthesis of Quinoxaline Derivatives via Copper(I)-Catalyzed Cross-Coupling Reaction of 1,2-Dihalobenzenes with N,N′-Disubstituted Ethane-1,2-diamines under Ligand- and Solvent-Free Conditions
    Shen, Guodong
    Zhao, Lingyu
    Zhao, Xiliang
    Huangfu, Xinlei
    Li, Zhe
    Wang, Rui
    Zhang, Tongxin
    SYNLETT, 2017, 28 (09) : 1111 - 1115
  • [27] Synthesis, Characterization, and Antimicrobial Evaluation of Sulfonamides Containing N-Acyl Moieties Catalyzed by Bismuth(III) Salts Under Both Solvent and Solvent-Free Conditions
    Adibi, Hadi
    Massah, Ahmad Reza
    Majnooni, Mohammad Bagher
    Shahidi, Sherita
    Afshar, Maryam
    Abiri, Ramin
    Naghash, Hamid Javaherian
    SYNTHETIC COMMUNICATIONS, 2010, 40 (18) : 2753 - 2766
  • [28] 1,3-Dibromo-5,5-dimethylhydantoin or N-bromosuccinimide as efficient reagents for chemoselective deprotection of 1,1-diacetates under solvent-free conditions
    Maleki, Behrooz
    Azarifar, Davood
    Ghorbani-vaghei, Ramin
    Veisi, Hojat
    Hojati, Seyedeh Fatemeh
    Gholizadeh, Mostafa
    Salehabadi, Hafezeh
    Khodaverdian, Mona
    Moghadam, Mona Khodaverdian
    MONATSHEFTE FUR CHEMIE, 2009, 140 (12): : 1485 - 1488
  • [29] 1,3-Dibromo-5,5-dimethylhydantoin or N-bromosuccinimide as efficient reagents for chemoselective deprotection of 1,1-diacetates under solvent-free conditions
    Behrooz Maleki
    Davood Azarifar
    Ramin Ghorbani-vaghei
    Hojat Veisi
    Seyedeh Fatemeh Hojati
    Mostafa Gholizadeh
    Hafezeh Salehabadi
    Mona Khodaverdian Moghadam
    Monatshefte für Chemie - Chemical Monthly, 2009, 140 : 1485 - 1488
  • [30] Selective Monobromination of 1,3-Diones with N-Bromosaccharin/Mg(ClO4)2 System in Solution and under Solvent-Free Conditions
    Alinezhad, Heshmatollah
    Tajbakhsh, Mahmood
    Tehrani, Shahram Shahriari
    BULLETIN OF THE KOREAN CHEMICAL SOCIETY, 2011, 32 (05) : 1543 - 1546
12345