New synthetic approach to peri-hydroxy-substituted carbonyl acenaphthene derivatives

被引：2
|
作者：
Bezuglov, A. N. [1 ]
Minyaeva, L. G. [1 ]
Mezheritskii, V. V. [1 ]
机构：
[1] So Fed Univ, Phys & Organ Chem Res Inst, Rostov Na Donu 344090, Russia
来源：
RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2008年 / 44卷 / 03期
关键词：
Sodium Methoxide; Steam Distillation; Dilute Hydrochloric Acid; Benzoyl Chloride; Raney Nickel;
D O I：
10.1134/S107042800803007X
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
A new approach to the synthesis of peri-hydroxyacenaphthoyl compounds has been developed on the basis of acylation (formylation) of 5-acyloxyacenaphthenes. The reactions are accompanied by formation of the corresponding 3- and 8-acyl-substituted isomers. In some cases, the latter can be isolated and identified by H-1 NMR spectroscopy.
引用
收藏
页码：353 / 357
页数：5
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