New synthetic approach to peri-hydroxy-substituted carbonyl acenaphthene derivatives

被引：2

作者：

Bezuglov, A. N. ^{[1
]}

Minyaeva, L. G. ^{[1
]}

Mezheritskii, V. V. ^{[1
]}

机构：

[1] So Fed Univ, Phys & Organ Chem Res Inst, Rostov Na Donu 344090, Russia

来源：

RUSSIAN JOURNAL OF ORGANIC CHEMISTRY | 2008年 / 44卷 / 03期

关键词：

Sodium Methoxide; Steam Distillation; Dilute Hydrochloric Acid; Benzoyl Chloride; Raney Nickel;

D O I：

10.1134/S107042800803007X

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A new approach to the synthesis of peri-hydroxyacenaphthoyl compounds has been developed on the basis of acylation (formylation) of 5-acyloxyacenaphthenes. The reactions are accompanied by formation of the corresponding 3- and 8-acyl-substituted isomers. In some cases, the latter can be isolated and identified by H-1 NMR spectroscopy.

引用

页码：353 / 357

页数：5

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