X-ray diffraction study, W-H plot, and Nelson-Relay function for the structural data of Ni0.7Zn0.3Fe2O4 + xwt%V2O5

被引:6
|
作者
Patil, Madhukar S. [1 ]
Patil, Aruna G. [2 ]
Barote, Vinod K. [3 ]
V. Raut, Anil [2 ]
Shengule, D. R. [2 ]
机构
[1] Yashvantrao Chavan Coll Sci, Dept Phys, Sillod 431112, Aurangabad, India
[2] Vivekanand Arts Sardar Dalipsingh Commerce & Sci C, Dept Phys, Aurangabad 431001, India
[3] St Dnyaneshwar Mahavidyalaya Soegaon, Dept Phys, Aurangabad 431120, India
关键词
X-ray diffraction; Additive; W-H plot; Nelson-Relay (N-R); Bradley-jay (B-J) extrapolation; FERRITE;
D O I
10.1016/j.matpr.2022.05.475
中图分类号
T [工业技术];
学科分类号
08 ;
摘要
In this study, we used the sol-gel method to make zinc doped nickel ferrite magnetic Ni0.7Zn0.3Fe2O4 + xwt%V2O5 (x = 0.0-1.0). The X-ray diffraction technique was used to examine the Ni0.7Zn0.3Fe2O4 + xwt%V2O5ferrite powder in order to identify Bragg's reflections and study the Miller indices (hkl). Using established formulas, the structural parameters lattice constant (a), unit cell volume (V), X-ray density (dx), porosity (P percent), and others have been calculated from XRD data. For the structural analysis, Bradley-jay (B-J) extrapolation (cos2h) versus lattice constant (a) was employed; also, Specimen misalignment (S-M) plot was used to describe the error-free values of lattice constant (a). To review the calculated crystallite size (D) and lattice constant, the Williamson-hall extrapolation function and Nelson-relay (N-R) extrapolation function were used (a). The results of the computations revealed cubic geometry, spinel structure, and Fd3m space group formation in Ni0.7Zn0.3Fe2O4 + xwt%V2O5 ferrite. In light of the significant uses of Ni0.7Zn0.3Fe2O4 + xwt%V2O5 in energy storage devices, microwave device technology, and magnetic applications, the prepared Ni0.7Zn0.3Fe2O4 + xwt%V2O5 might be regarded for further research by the research community. Copyright (C) 2022 Elsevier Ltd. All rights reserved.
引用
收藏
页码:123 / 127
页数:5
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