Ultrasound-assisted one-pot synthesis of α-oxycarbanilinophosphonates via a three-component condensation of an aldehyde, diethyl phosphite and an isocyanate under solvent-free conditions

被引：14
|
作者：
Kaboudin, Babak [1 ]
Fallahi, Maryam [1 ]
机构：
[1] Inst Adv Studies Basic Sci IASBS, Dept Chem, Gava Zang 4513766731, Zanjan, Iran
来源：
TETRAHEDRON LETTERS | 2011年 / 52卷 / 33期
关键词：
ANTIBODY-CATALYZED HYDROLYSIS; AMMONIUM HYDROGEN CARBONATE; PHOSPHONIC ACID ANALOGS; LI-BINOL COMPLEX; MICROWAVE IRRADIATION; ASYMMETRIC-SYNTHESIS; EFFICIENT REAGENT; ORGANIC-CHEMISTRY; ORGANOPHOSPHORUS COMPOUNDS; CONVENIENT SYNTHESIS;
D O I：
10.1016/j.tetlet.2011.06.057
中图分类号：
O62 [有机化学];
学科分类号：
070303 ; 081704 ;
摘要：
An efficient one-pot method has been developed for the synthesis of alpha-oxycarbanilinophosphonates via a one-pot reaction of an aldehyde with diethyl phosphite in the presence of magnesium oxide followed by reaction with an isocyanate under solvent-free conditions using ultrasonic irradiation. This method is simple, rapid and good yielding. (C) 2011 Elsevier Ltd. All rights reserved.
引用
收藏
页码：4346 / 4348
页数：3
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