Methyl 2,2′-dimethyl-4′-[2-(methylsulfanyl)ethyl]-1,3-dioxo-2,3-dihydro-1H,4′H-spiro[isoquinoline-4,5′-oxazole]-4′-carboxylate

被引：0

作者：

Fun, Hoong-Kun ^{[1
]}

Quah, Ching Kheng ^{[1
]}

Huang, Chengmei ^{[2
]}

Yu, Haitao ^{[2
]}

机构：

[1] Univ Sains Malaysia, Xray Crystallog Unit, Sch Phys, Usm 11800, Penang, Malaysia

[2] Nanjing Univ, Sch Chem & Chem Engn, Nanjing 210093, Peoples R China

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE | 2011年 / 67卷

关键词：

X-RAY; DIFFRACTION; INHIBITORS; DISCOVERY;

D O I：

10.1107/S1600536811030133

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the isoquinoline ring system of the title molecule, C18H20N2O5S, the fused N-heterocyclic ring is distorted towards a half-boat conformation. The methyl formate moiety is disordered over two sets of sites with refined occupancies of 0.882 (5) and 0.118 (5). In the crystal, molecules are linked via weak intermolecular C-H center dot center dot center dot O hydrogen bonds into one-dimensional chains along [010].

引用

页码：O2216 / U1579

页数：13

共 50 条

[31] An efficient synthesis of 1',4'-dihydro-2'H-spiro[azetidin-2,3'-quinolin]-2'-one
Huang, Longjiang
Tian, Yuan
Teng, Dawei
RESEARCH ON CHEMICAL INTERMEDIATES, 2017, 43 (01) : 219 - 228
[32] Two-step novel synthesis of 2-amino-6-(1,3-dioxo-2,3-dihydro-1H-inden-2-yl)-4,7-diphenyloxepine-3-carbonitrile and 5-(1,3-dioxo-2,3-dihydro-1H-inden-2-yl)-2-imino-6-phenyl-2H-pyran-3-carbonitrile
Abou Elmaaty, Tarek M.
SYNTHETIC COMMUNICATIONS, 2006, 36 (16) : 2281 - 2285
[33] Ethyl 1-(2-hydroxyethyl)-2-[2-(methylsulfanyl)ethyl]-1H-benzimidazole-5-carboxylate
Hamzah, Nurasyikin
Ngah, Nurziana
Hamid, Shafida Abd
Rahim, Aisyah Saad Abdul
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2012, 68 : o197 - o198
[34] 4-[(1,3-Dioxo-2,3-dihydro-1H-benzo-[de]isoquinolin-2-yl)methyl]-N′-[(E)-4-nitrobenzylidene]benzenesulfono-hydrazide dimethyl sulfoxide monosolvate
Bortoluzzi, Adailton J.
Policarpi, Everton B.
Mora, Cristiano
Oliveira, Kely N.
Nunes, Ricardo J.
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O627 - U1795
[35] 2-(2-methoxyphenyl)-4,4-dimethyl-4,5dihydro-1,3-oxazole
Thiruvalluvar, A.
Butcher, Ray J.
Karegoudar, Prakash
Holla, B. Shivarama
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2008, 64 : O61 - U3054
[36] Single crystal X-ray structure of 2-[({[(4-methylphenyl)sulfonyl]methyl} amino)carbonyl]-1,3-dioxo-2,3-dihydro-1H-inden-2-yl 2-thiophenecarboxylate
Ramazani, A.
Kazemizadeh, A. R.
Slepokura, K.
Lis, T.
JOURNAL OF STRUCTURAL CHEMISTRY, 2011, 52 (06) : 1085 - 1090
[37] Single crystal X-ray structure of 2-[({[(4-methylphenyl)sulfonyl]methyl} amino)carbonyl]-1,3-dioxo-2,3-dihydro-1H-inden-2-yl 2-thiophenecarboxylate
A. Ramazani
A. R. Kazemizadeh
K. Ślepokura
T. Lis
Journal of Structural Chemistry, 2011, 52 : 1085 - 1090
[38] Ethyl 4-anilino-2-methyl-5-oxo-1-phenyl-2,5-dihydro-1H-pyrrole-2-carboxylate
Akkurt, Mehmet
Mohamed, Shaaban K.
Elremaily, Mahmoud A. A.
Santoyo-Gonzalez, Francisco
Albayati, Mustafa R.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : O1757 - +
[39] 2-(4-Methoxyphenyl)-4,5-dihydro-1H-imidazole
Kia, Reza
Fun, Hoong-Kun
Kargar, Hadi
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2009, 65 : O798 - U2367
[40] Ethyl 1-[2-(morpholin-4-yl)ethyl]-2-[4(trifluoromethyl)phenyl]-1H-benzimidazole-5-carboxylate
Yoon, Yeong Keng
Ali, Mohamed Ashraf
Choon, Tan Soo
Hemamalini, Madhukar
Fun, Hoong-Kun
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2011, 67 : O1215 - U1249

← 1 2 3 4 5 →