Synthesis and crystal structure of (S)-(+)-2-[(1,1-dimethylethoxy)carbonyl]amino-2-phenylethanol

被引：1
|
作者：
Sperandio, C [1 ]
Denis, JN [1 ]
Averbuch-Pouchot, MT [1 ]
Vallee, Y [1 ]
机构：
[1] Univ Grenoble 1, Etud Dynam & Struct Select Lab, CNRS, F-38041 Grenoble 9, France
来源：
COMPTES RENDUS DE L ACADEMIE DES SCIENCES SERIE II FASCICULE C-CHIMIE | 1998年 / 1卷 / 11期
关键词：
crystal structure; beta-amino alcohols; synthetic intermediates; (S)-(+)-2-phenylglycinol;
D O I：
10.1016/S1387-1609(99)80027-9
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
The preparation and the crystal structure of the title compound are described. C(6)H(5)CH[NHCOOC(CH(3))(3)]CH(2)OH is monoclinic with the following unit-cell dimensions: a = 10.354(2), b = 6.533(3), c = 10.505(1) Angstrom, beta = 38.58(1)degrees. The space group is P2(1) and Z = 2. The crystal-structure determination was run by using 1481 independent reflexions with a final R value of 0.033 (R(w) = 0.043). (C) Academie des sciences/Elsevier, Paris.
引用
收藏
页码：709 / 714
页数：6
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