ToF-SIMS and XPS study of ancient papers

被引：8
|
作者：
Benetti, Francesca [1 ]
Marchettini, Nadia [1 ]
Atrei, Andrea [1 ]
机构：
[1] Univ Siena, Dipartimento Chim, I-53100 Siena, Italy
来源：
APPLIED SURFACE SCIENCE | 2011年 / 257卷 / 06期
关键词：
ToF-SIMS; XPS; Ancient paper; Surface analysis; GELATIN; DISCOLORATION; SPECTROSCOPY; SPECTROMETRY;
D O I：
10.1016/j.apsusc.2010.09.063
中图分类号：
O64 [物理化学（理论化学）、化学物理学];
学科分类号：
070304 ; 081704 ;
摘要：
The surface composition of 18th century papers was investigated by means of ToF-SIMS and XPS. The aim of the present study was to explore the possibility of using these surface sensitive methods to obtain information which can help to determine the manufacturing process, provenance and state of conservation of ancient papers. The ToF-SIMS results indicate that the analyzed papers were sized by gelatin and that alum was added as hardening agent. The paper sheets produced in near geographical areas but in different paper mills exhibit a similar surface composition and morphology of the fibers as shown by the ToF-SIMS measurements. The ToF-SIMS and the XPS results indicate that a significant fraction of the cellulose fibers is not covered by the gelatin layer. This was observed for the ancient papers and for a modern handmade paper manufactured according to the old recipes. (C) 2010 Elsevier B.V. All rights reserved.
引用
收藏
页码：2142 / 2147
页数：6
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