ONE-POT, THREE-COMPONENT SYNTHESIS OF α-AMINO PHOSPHONATES USING NaHSO4-SiO2 AS AN EFFICIENT AND REUSABLE CATALYST

被引：18

作者：

Maghsoodlou, Malek Taher ^{[1
]}

Heydari, Reza ^{[1
]}

Habibi-Khorassani, Sayyed Mostafa ^{[1
]}

Hazeri, Nourallah ^{[1
]}

Sajadikhah, Seyed Sajad ^{[1
]}

Rostamizadeh, Mohsen ^{[1
]}

Lashkari, Mojtaba ^{[1
]}

机构：

[1] Univ Sistan & Baluchestan, Dept Chem, Fac Sci, Zahedan, Iran

来源：

SYNTHETIC COMMUNICATIONS | 2012年 / 42卷 / 01期

关键词：

alpha-Amino phosphonates; heterogeneous catalyst; NaHSO4-SiO2; reusable catalyst; trialkylphosphite; ORGANIC PHOSPHORUS-COMPOUNDS; ENANTIOSELECTIVE SYNTHESIS; ACID; INHIBITORS; AMINOPHOSPHONATES; ALDEHYDES; PROTOCOL; WELL;

D O I：

10.1080/00397911.2010.523153

中图分类号：

O62 [有机化学];

学科分类号：

070303 ; 081704 ;

摘要：

A simple, efficient, and environmentally benign method has been developed for the synthesis of alpha-amino phosphonates. One-pot, three-component reaction of aldehyds, amines, and trialkylphosphite in the presence of silica-supported sodium hydrogen sulfate (NaHSO4-SiO2) as an inexpensive and reusable catalyst under solvent-free conditions at 80 degrees C affords the corresponding a-amino phosphonates in good yields and short reaction times.

引用

页码：136 / 143

页数：8

共 50 条

[1] SiO2-NaHSO4 as an Efficient Reusable Heterogeneous Catalyst for the One-Pot Three-Component Synthesis of Octahydro-quinazolin-2,5-diones in Water
Azzam, Sadeq Hamood Saleh
Siddekha, Aisha
Nizam, Aatika
Pasha, Mohamed Afzal
[J]. CHINESE JOURNAL OF CATALYSIS, 2012, 33 (04) : 677 - 680
[2] Al(H2PO4)3 as an Efficient and Reusable Catalyst for One-pot Three-component Synthesis of α-Amino Phosphonates under Solvent-free Conditions
Maghsoodlou, Malek Taher
Habibi-Khorassani, Sayyed Mostafa
Heydari, Reza
Hazeri, Nourollah
Sajadikhah, Seyed Sajad
Rostamizadeh, Mohsen
[J]. CHINESE JOURNAL OF CHEMISTRY, 2010, 28 (02) : 285 - 288
[3] -functionalized magnetic nanoparticles as an efficient and reusable catalyst for one-pot synthesis of -amino phosphonates
Hamadi, Hosein
Norouzi, Meysam
[J]. JOURNAL OF CHEMICAL SCIENCES, 2018, 130 (09)
[4] One-pot three-component synthesis of α-amino nitriles using ZnO as a heterogeneous, reusable, and eco-friendly catalyst
Kaur, Balwinder
Chand, Subhash
Malik, Ashok Kumar
Dhaliwal, Karamjit Singh
Younis, Sherif A.
Kim, Ki-Hyun
[J]. JOURNAL OF CLEANER PRODUCTION, 2019, 234 : 329 - 339
[5] Three-component one-pot synthesis of α-hydroxylamino phosphonates using ionic liquids
Yadav, JS
Reddy, BVS
Sreedhar, P
[J]. ADVANCED SYNTHESIS & CATALYSIS, 2003, 345 (05) : 564 - 567
[6] Silica supported polyphosphoric acid (PPA-SiO2): an efficient and reusable heterogeneous catalyst for the one-pot synthesis of α-amino phosphonates
Maghsoodlou, Malek Taher
Khorassani, Sayyed Mostafa Habibi
Heydari, Reza
Hazeri, Nourollah
Sajadikhah, Seyed Sajad
Rostamizadeh, Mohsen
Keishams, Leila
[J]. TURKISH JOURNAL OF CHEMISTRY, 2010, 34 (04) : 565 - 570
[7] Ketones in the catalytic three-component “one-pot” Kabachnik-Fields synthesis of α-amino phosphonates
E. D. Matveeva
T. A. Podrugina
M. V. Prisyajnoy
N. S. Zefirov
[J]. Russian Chemical Bulletin, 2006, 55 : 1209 - 1214
[8] A green protocol for one-pot three-component synthesis of α-amino phosphonates catalyzed by succinic acid
Nourallah Hazeri
Malek Taher Maghsoodlou
Sayyed Mostafa Habibi-Khorassani
Jasem Aboonajmi
Mojtaba Lashkari
Seyed Sajad Sajadikhah
[J]. Research on Chemical Intermediates, 2014, 40 : 1781 - 1788
[9] Amberlite-IR 120 catalyzed three-component synthesis of α-amino phosphonates in one-pot
Bhattacharya, Asish K.
Rana, Kalpeshkumar C.
[J]. TETRAHEDRON LETTERS, 2008, 49 (16) : 2598 - 2601
[10] A green protocol for one-pot three-component synthesis of α-amino phosphonates catalyzed by succinic acid
Hazeri, Nourallah
Maghsoodlou, Malek Taher
Habibi-Khorassani, Sayyed Mostafa
Aboonajmi, Jasem
Lashkari, Mojtaba
Sajadikhah, Seyed Sajad
[J]. RESEARCH ON CHEMICAL INTERMEDIATES, 2014, 40 (05) : 1781 - 1788

← 1 2 3 4 5 →