Determination of volatile compounds in whiting (Merlangius merlangus) using headspace-solid-phase microextraction-gas chromatography-mass spectrometry

被引：17
|
作者：
Duflos, G [1 ]
Moine, F [1 ]
Coin, VM [1 ]
Malle, P [1 ]
机构：
[1] Agence Francaise Secur Sanitaire Aliments, Lab Etude & Rech Produits Peche, F-62200 Boulogne, France
来源：
JOURNAL OF CHROMATOGRAPHIC SCIENCE | 2005年 / 43卷 / 06期
关键词：
D O I：
10.1093/chromsci/43.6.304
中图分类号：
Q5 [生物化学];
学科分类号：
071010 ; 081704 ;
摘要：
A method using headspace-solid-phase microextraction-gas chromatography-mass spectrometry to extract volatile compounds from whiting is developed. Several parameters such as sorption time, desorption time, fiber type, and matrix form are optimized to achieve better sensitivity in minimal analysis time. The efficiency of the method is determined by the linear range and repeatability; a mean relative standard deviation of approximately 7% is measured. It was possible to identify and quantitate 30 volatile compounds of interest present in spoiled whiting.
引用
收藏
页码：304 / 312
页数：9
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